Effect of tantalum addition on the mechanical properties of tungsten/tantalum composite thin films

Tungsten (W) when used as a plasma-facing material (PFM) in a tokamak will face harsh neutron radiation and high-temperature fluctuations. Due to its ductile-to-brittle transition temperature (DBTT), W behaves as a brittle material in lower temperatures and thus helps in propagating cracks easily resulting in dust formation and failure of material. In this study, an attempt has been made to improve the ductility, hardness, and toughness of W thin films by adding tantalum (Ta) to it, resulting in composite thin films. W/Ta composite thin films deposited on reduced-activation ferritic martensitic steel (RAFM) steel by RF magnetron sputtering method are compared with W thin films deposited on the same substrate. Taguchi orthogonal array is used to get the best properties for the composite thin films and nanoindentation technique is used to evaluate the mechanical properties of developed thin films. With the least hardness of 7.19 Gpa, composite film hardness is 452% lesser than the maximum hardness of (39.54 Gpa) W films. The reduction in hardness for composite thin films has not depleted the toughness as the E-f/E-s ratio is higher than cracking threshold of 1.3. The maximum plastic energy absorbed for yield by composite films during nanoindentation is (1710 mN nm) 14% higher than W thin film (1500 mN nm), indicating the composite film is a ductile and tougher than the W film.