Barium Hydroxyapatite Ba10(PO4)6(OH)2 and Barium Nitrate: New Recyclable Catalysts for the Synthesis of 3,4-dihydropyrimidin-2(1H)-ones/thiones

被引:0
|
作者
Lachheb, Jalel [1 ]
Ben Moussa, Sana [2 ]
Mehri, Afef [1 ]
Badraoui, Bechir [1 ]
机构
[1] Univ Monastir, Preparatory Inst Engn Studies Monastir, UR Mat & Organ Synth UR 17ES31, Monastir 5019, Tunisia
[2] King Khalid Univ, Fac Sci & Arts, Mahail Assir, Saudi Arabia
来源
JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN | 2023年 / 45卷 / 05期
关键词
Dihydropyrimidinones; Multi-component reactions (MCRs); Biginelli reaction; Barium hydroxyapatite (BaHAp); Recyclable catalyst; ONE-POT SYNTHESIS; HETEROGENEOUS CATALYST; EFFICIENT SYNTHESIS; BIGINELLI REACTION; LEWIS-ACID; 3,4-DIHYDROPYRIMIDIN-2-(1H)-ONES; NANOPARTICLES; INHIBITORS; THIONES;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In this paper, we report an efficient synthesis of 3,4-dihydropyrimidin-2(1H)-ones/thiones (DHPMs) from the Biginelli condensation reaction of ethyl acetoacetate, aromatic aldehydes and urea or thiourea catalysed by barium (II) nitrate and barium hydroxyapatite Ba10(PO4)6(OH)2 (BaHAp). These new catalysts exhibited an important reactivity and proved reusable
引用
收藏
页码:453 / 459
页数:7
相关论文
共 50 条
  • [41] Hypervalent iodine(III) reagent in the solid-state synthesis of 3,4-dihydropyrimidin-2(1H)-ones
    Pundeer, Rashmi
    Sushma
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2015, 54 (10): : 1275 - 1279
  • [42] Preparation of 6-Unsubstituted 3,4-Dihydropyrimidin-2(1H)-Ones and 2-(Arylamino)Pyrimidines
    Terentjeva, S.
    Muceniece, D.
    Lusis, V.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2014, 49 (12) : 1757 - 1769
  • [43] ULTRASOUND-MEDIATED SYNTHESIS OF 3,4-DIHYDROPYRIMIDIN-2-(1H)-ONES (OR THIONES) WITH NaHSO4•H2O
    Dilmaghani, Karim Akbari
    Zeynizadeh, Behzad
    Amirpoor, Maryam
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2013, 188 (11) : 1634 - 1642
  • [44] Sodium alginate: A renewable and very effective biopolymer catalyst for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones
    Daemi, H.
    Rad, R. Rezaieyeh
    Adib, M.
    Barikani, M.
    SCIENTIA IRANICA, 2014, 21 (06) : 2076 - 2081
  • [45] BiVO4-NPs: an efficient nano-catalyst for the synthesis of biscoumarins, bis(indolyl)methanes and 3,4-dihydropyrimidin-2(1H)-ones (thiones) derivatives
    Shirini, Farhad
    Lati, Monireh Pourghasemi
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2017, 14 (01) : 75 - 87
  • [46] Synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by poly(ferric 2-acrylamido-2-methylpropanesulfonate)
    Zhao, Zhihao
    Dai, Hongguang
    Shi, Lan
    CHEMICAL PAPERS, 2021, 75 (02): : 583 - 590
  • [47] Synthesis of 3,4-Dihydropyrimidin-2(1H)-one Derivatives Using Activated Montmorillonite as Catalyst
    Mekki, Sofiane
    Krabia, Lahcen
    Mohamed, Saleh Mahmoud Saleh
    Saidi-Besbes, Salima
    LETTERS IN ORGANIC CHEMISTRY, 2019, 16 (01) : 59 - 65
  • [48] Chloroferrate(III) ionic liquid:: Efficient and recyclable catalyst for solvent-free synthesis of 3,4-dihydropyrimidin-2(1H)-ones
    Chen, Xiaofen
    Peng, Yanqing
    CATALYSIS LETTERS, 2008, 122 (3-4) : 310 - 313
  • [49] Chloroferrate(III) Ionic Liquid: Efficient and Recyclable Catalyst for Solvent-free Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones
    Xiaofen Chen
    Yanqing Peng
    Catalysis Letters, 2008, 122 : 310 - 313
  • [50] One-pot synthesis of 3,4-Dihydropyrimidin-2(1H)-ones (thiones) promoted by nano-BF3.SiO2
    B. F. Mirjalili
    A. Bamoniri
    A. Akbari
    Journal of the Iranian Chemical Society, 2011, 8 : S135 - S140