Optimization of nano cellulose extraction from timoho fiber using response surface methodology (RSM)

被引：14
|
作者：
Diharjo, Kuncoro [1 ]
Gapsari, Femiana [2 ]
Andoko, Andoko [3 ]
Septiari, Renny [4 ]
Rangappa, Sanjay Mavinkere [5 ]
Siengchin, Suchart [5 ]
机构：
[1] Sebelas Maret Univ, Fac Engn, Mech Engn Dept, Ir Sutami 36, Surakarta 57126, Indonesia
[2] Brawijaya Univ, Fac Engn, Mech Engn Dept, MT Haryono 167, Malang 65145, Indonesia
[3] State Univ Malang, Fac Engn, Mech Engn Dept, Semarang 5, Malang 65145, Indonesia
[4] Natl Inst Technol ITN, Fac Engn, Dept Ind Engn, Malang 65145, Indonesia
[5] King Mongkuts Univ Technol North Bangkok KMUTNB, Sirindhorn Int Thai German Grad Sch Engn TGGS, Dept Mat & Prod Engn, Nat Composites Res Grp Lab, Bangkok, Thailand
来源：
BIOMASS CONVERSION AND BIOREFINERY | 2023年 / 14卷 / 20期
关键词：
Hydrolysis; Nano cellulose; RSM; Timoho fiber; MICROCRYSTALLINE CELLULOSE; NANOCRYSTALS; NANOCELLULOSE; HYDROLYSIS;
D O I：
10.1007/s13399-023-04551-9
中图分类号：
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号：
0807 ; 0820 ;
摘要：
Hydrolysis process involves determining the parameters of the sulfuric acid concentration and exact mixing time and temperature. To optimize the nano cellulose yield from timoho fiber (TF), an experimental design was carried out using response surface methodology (RSM) to obtain a combination of hydrolysis process parameters resulting in maximum nano cellulose. The combination of 37.5% H2SO4 at 45(degrees)C for 90 min produced the maximum nano cellulose yield of 84.95%. The combination of parameters was confirmed and characterized using thermal analysis, FTIR FE-SEM, XRD, and TEM. The combination result of process parameters in this study could be used as a reference in nano cellulose production using hydrolysis.
引用
收藏
页码：25557 / 25567
页数：11
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