Determination of restricted dyes in textile raw material solid wastes by ultra-high performance liquid chromatography-tandem mass spectrometry

被引:4
作者
Sun, Qianran [1 ]
Li, Yongli [1 ]
Su, Youzhi [2 ]
Wei, Mengyuan [3 ]
Li, Haitao [4 ]
Liu, Jun [1 ,5 ,6 ]
机构
[1] Chengdu Customs Dist, Technol Ctr, Chengdu 610000, Peoples R China
[2] Yining Customs Dist, Technol Ctr, Yining 835000, Peoples R China
[3] Shanghai Customs Dist, Shanghai 200135, Peoples R China
[4] Tianjin Phys & Chem Anal Ctr Co LTD, Tianjin 300051, Peoples R China
[5] Urumqi Customs Dist, Urumqi 830000, Peoples R China
[6] Chengdu Customs, Technol Ctr, 28, Yihuan Rd, Chengdu 611430, Peoples R China
关键词
Restricted dyes; UHPLC-MS/MS; Textile raw material solids waste; Ultrasonic extraction; DISPERSE DYES; ION SUPPRESSION; WATER; ELECTROSPRAY; EXTRACTION; THROUGHPUT; PRODUCTS; AZO;
D O I
10.1016/j.chroma.2023.464447
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A rapid and highly sensitive method for the quantification of 34 restricted dyes (including acid, basic, disperse, direct, and azo dyes) in solid textile raw material wastes was developed by employing ultrasonic extraction coupled with ultra-high performance liquid chromatography-tandem mass spectrometry(UHPLC-MS/MS). More specifically, the proposed method employed methanol as the extraction solvent, while the mobile phases consisted of acetonitrile and 10 mmol/L ammonium acetate + 0.05% ammonia. A good linearity was achieved over the concentration range of 0.01-200 ng/mL with correlation coefficients (R) between 0.991-0.999, limits of detection (LODs) of 0.25-40.0 mu g/kg (S/N = 3) and limits of quantification (LOQs) of 0.84-133.4 mu g/kg (S/N = 10). 34 dyes were recovered at three levels ranging from 84.5 to 106.9% with relative standard deviation (RSDs) ranging from 0.59% to 10.61%. Further, the method was applied for the accurate analysis of 32 counts of cotton yarn, waste cotton, and printed fabrics within 15 min. The dyestuffs accurately quantified by this rapid chromatographic procedure covered a wide range of carcinogenic and allergenic dyestuffs listed in the Oeko-Tex Standard 100 (version 02.2023) colourants. The ultrasound technique combined with the ultra-high performance liquid chromatography-tandem mass spectrometry method proposed in this work is thus suitable for the rapid screening, confirmation, and quantitative detection of industrial synthetic dyes within solid waste originating from textile raw materials.
引用
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页数:13
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