New magnetic nanocomposite Fe3O4@Saponin/Cu(II) as an effective recyclable catalyst for the synthesis of aminoalkylnaphthols via Betti reaction

被引:3
作者
Heidarpour, Majid [1 ]
Kiani, Marziyeh [1 ]
Anaraki-Ardakani, Hossein [2 ]
Rezaei, Parizad [3 ]
Ghaleh, Saeed Parvizi [4 ]
Ahmadi, Reza [5 ]
Maleki, Mohammad [1 ]
机构
[1] Islamic Azad Univ, Dept Chem, Ahvaz Branch, Ahvaz, Iran
[2] Islamic Azad Univ, Dept Chem, Mahshahr Branch, Mahshahr, Iran
[3] Islamic Azad Univ, Dept Chem Engn, Abadan Branch, Abadan, Iran
[4] Sahand Univ Technol, Fac Petr & Nat Gas Engn, Tabriz, Iran
[5] Islamic Azad Univ, Dept Environm Engn, West Tehran Branch, Tehran, Iran
关键词
Green chemistry; Saponin; Three-component; copper(II) chloride; ONE-POT SYNTHESIS; SOLVENT-FREE; REUSABLE CATALYST; NONIONIC SURFACTANT; EFFICIENT SYNTHESIS; BASES; ACID; 1-AMIDOALKYL-2-NAPHTHOLS; NANOPARTICLES; DERIVATIVES;
D O I
10.1016/j.steroids.2022.109170
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
In this research, a new magnetic nanocomposite Fe3O4@Saponin/Cu(II) based on quillaja saponin was prepared and the catalyst structure was characterized thoroughly using FT-IR, EDS, TGA, XRD, VSM, HR-TEM, SEM, ICP, BET analyzes. The catalyst prepared in the three-component synthesis of several Betti bases, 1-(alpha-aminoalkyl) naphthols, under environmentally friendly conditions was used. The advantage of this reaction is the high ef-ficiency of the products and the short reaction time. Furthermore, Fe3O4@Saponin/Cu(II) nano-catalyst is recoverable magnetically and is reusable for other processes with no reduction in its activity.
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页数:13
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