The Effect of Annealing on the Soft Magnetic Properties and Microstructure of Fe82Si2B13P1C3 Amorphous Iron Cores

被引:1
作者
Zheng, Wei [1 ,2 ,3 ]
Zhang, Guangqiang [3 ]
Zhang, Qian [1 ,2 ]
Yu, Haichen [4 ]
Li, Zongzhen [3 ]
Gu, Mingyu [5 ]
Song, Su [3 ]
Zhou, Shaoxiong [2 ,3 ]
Qu, Xuanhui [1 ]
机构
[1] Univ Sci & Technol Beijing, Inst Adv Mat & Technol, Beijing 100083, Peoples R China
[2] Cent Iron & Steel Res Inst, Beijing 100081, Peoples R China
[3] Jiangsu JITRI Adv Energy Mat Res Inst Co Ltd, Changzhou 213001, Peoples R China
[4] North China Elect Power Univ, Inst Adv Mat, Beijing 102206, Peoples R China
[5] Shandong Univ, Elect & Informat Engn, Weihai 264209, Peoples R China
基金
中国国家自然科学基金;
关键词
amorphous iron core; magnetic field annealing; core loss; domains; HIGH B-S; ALLOYS; MOTOR; IMPROVEMENT; GLASS;
D O I
10.3390/ma16165527
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
This research paper investigated the impact of normal annealing (NA) and magnetic field annealing (FA) on the soft magnetic properties and microstructure of Fe82Si2B13P1C3 amorphous alloy iron cores. The annealing process involved various methods of magnetic field application: transverse magnetic field annealing (TFA), longitudinal magnetic field annealing (LFA), transverse magnetic field annealing followed by longitudinal magnetic field annealing (TLFA) and longitudinal magnetic field annealing followed by transverse magnetic field annealing (LTFA). The annealed samples were subjected to testing and analysis using techniques such as differential scanning calorimetry (DSC), transmission electron microscopy (TEM), X-ray diffraction (XRD), magnetic performance testing equipment and magneto-optical Kerr microscopy. The obtained results were then compared with those of commercially produced Fe80Si9B11. Fe82Si2B13P1C3 demonstrated the lowest loss of P-1.4T,P-2kHz = 8.1 W/kg when annealed in a transverse magnetic field at 370 degrees C, which was 17% lower than that of Fe80Si9B11. When influenced by the longitudinal magnetic field, the magnetization curve tended to become more rectangular, and the coercivity (B-3500A/m) of Fe(82)Si(2)B(13)P(1)C(3 )reached 1.6 T, which was 0.05 T higher than that of Fe80Si9B11. During the 370 degrees C annealing process of the Fe82Si2B13P1C3 amorphous iron core, the internal stress in the strip gradually dissipated, and impurity domains such as fingerprint domains disappeared and aligned with the length direction of the strip. Consequently, wide strip domains with low resistance and easy magnetization were formed, thereby reducing the overall loss of the amorphous iron core.
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页数:13
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