Development of anisotropic Nd-Fe-B powder from isotropic gas atomized powder

This work presents an innovative approach to obtain anisotropic Nd-Fe-B powder from isotropic gas atomized powder. The new process was developed using a ternary Nd-Fe-B alloy, without the requirement for additional heavy rare earth or other critical raw materials. It comprises the following steps: (a) gas atomization to produce a polycrystalline isotropic powder; (b) annealing at high temperature to induce grain growth; (c) hydrogen decrepitation to obtain a monocrystalline powder; and (d) hydrogenation-disproportionation-desorptionrecombination to obtain the final ultrafine anisotropic particles. The final particle shape is polygonal, which should improve the injection molding characteristics of current powder. The final powder exhibits both high remanence (0.97 T) and coercivity (1354 kA/m) for laboratory batch sizes, which is a result of its anisotropic ultrafine microstructure. Thus, gas atomization is considered a feasible alternative to casting methods as a first step to produce powders for anisotropic bonded magnet.