Influence of Temperature on the Growth of Vertically Aligned ZnO Nanowires in Wet Oxygen Environment

被引:3
作者
ElZein, Basma [1 ,2 ]
Salah, Numan [3 ]
Barham, Ahmad S. [4 ]
Elrashidi, Ali [1 ,5 ]
Al Khatab, Mohammed [1 ]
Jabbour, Ghassan [6 ]
机构
[1] Univ Business & Technol, Coll Engn, Jeddah 21361, Saudi Arabia
[2] Global Council Tolerance & Peace, Sustainable Dev, VLT1011, Valletta, Malta
[3] King Abdulaziz Univ, Ctr Nanotechnol, Jeddah 21589, Saudi Arabia
[4] Univ Jordan, Dept Chem, Amman 11942, Jordan
[5] Alexandria Univ, Dept Engn Phys, Alexandria 21544, Egypt
[6] Univ Ottawa, Adv Mat & Devices Labs, 75 Laurier Ave E, Ottawa, ON K1N 6N5, Canada
关键词
wet oxidation; ZnO NWs; n-type silicon substrate; zinc seed layer; oxygen rich environment; water vapor; thermal evaporation; ZINC-OXIDE; THIN-FILMS; THERMAL-OXIDATION; NANOSTRUCTURES; VAPOR; FABRICATION;
D O I
10.3390/cryst13060876
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The nanowires (NWs) of zinc oxide (ZnO) are developed effectively on an n-type silicon substrate through a seed zinc (Zn) layer by a wet oxidation technique. The growth is performed at different temperatures, 650, 750, and 850 & DEG;C, in a wet and rich oxygen environment under a flow of oxygen in the presence of water vapor at atmospheric pressure with a heating rate of 100 & DEG;C in 30 min. At 415 & DEG;C, the oxygen gas is introduced for the oxidation process. The Zn seed layer is deposited by the thermal evaporation technique. The structural, morphological, and optical properties are investigated. The temperature effect on NWs of ZnO growth intensity and their direction are explored. The nanowires are grown vertically oriented at a temperature of T = 750 & DEG;C. The ultraviolet (UV) analysis has been exposed in the visible region ranging from 10 nm to 700 nm at UV to visible intensity ratio of 2.22. In addition, X-ray diffraction analysis (XRD) is employed to research the structural properties of NWs of ZnO, and the characterization is verified by a scanning electron microscope (SEM) to investigate the morphology.
引用
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页数:12
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