Effect of two-step sintering on microstructure and mechanical properties of ceria-stabilized zirconia-toughened alumina-added titania (CSZTA-TiO2)

被引:1
作者
Eggidi, Obulapathi [1 ]
Pandey, Ajoy Kumar [1 ]
机构
[1] Natl Inst Technol, Dept Met & Mat Engn, Warangal 506004, Andhra Pradesh, India
关键词
CSZTA-TiO2; fracture toughness; two-step sintering; GRAIN-SIZE; MONOCLINIC TRANSFORMATION; FRACTURE-TOUGHNESS; PHASE-STABILITY; TIO2; ADDITION; CERAMIC TOOL; DENSIFICATION; TEMPERATURE; STRENGTH; BEHAVIOR;
D O I
10.1111/ijac.14203
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Effect of two-step sintering (TSS) on microstructure and mechanical properties of ceria-stabilized zirconia-toughened alumina with added TiO2 (CSZTA-TiO2) was studied. A coprecipitation technique was used to produce the CSZTA-TiO2 powders. The synthesized powders were compacted using a uniaxial hydraulic press and conventionally sintered in air. The phase and microstructure of sintered samples were studied using X-ray diffraction and scanning electron microscopy techniques. Phases were quantified using the Rietveld refinement method. Different TSS schedules were followed to optimize microstructure and mechanical properties. Mechanical properties of the CSZTA-4TiO(2) composite were evaluated and found as follows: Vickers's hardness of 1650 +/- 9.6 HV10, indentation fracture toughness of 8.45 +/- .14 MPa root m, compressive strength of 2088 MPa, and Young's modulus of 158 GPa.
引用
收藏
页码:294 / 305
页数:12
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