Phase imaging in scanning transmission electron microscopy using bright-field balanced divergency method

被引:2
作者
Wang, Binbin [1 ,2 ,3 ]
McComb, David W. [1 ,2 ]
机构
[1] Ohio State Univ, Ctr Electron Microscopy & Anal, Columbus, OH 43212 USA
[2] Ohio State Univ, Mat Sci & Engn, Columbus, OH 43212 USA
[3] Intel Corp, Hillsboro, OR 97124 USA
关键词
Phase retrieval; TEM; Atomic resolution; Magnetic; electric field; Direct detector; CONTRAST;
D O I
10.1016/j.ultramic.2022.113665
中图分类号
TH742 [显微镜];
学科分类号
摘要
We introduce a phase imaging mechanism for scanning transmission electron microscopy that exploits the complementary intensity changes of transmitted disks at different scattering angles. For scanning transmission electron microscopy, this method provides a straightforward, dose-efficient, and noise-robust phase imaging, from atomic resolution to intermediate length scales, as a function of scattering angles and probe defocus. At atomic resolution, we demonstrate that the phase imaging using the method can detect both light and heavy atomic columns. Furthermore, we experimentally apply the method to the imaging of nanoscale magnetic phases in FeGe samples. Compared with conventional methods, phase retrieval using the new method has higher effective spatial resolution and robustness to non-phase background contrast. Our method complements tradi-tional phase imaging modalities in electron microscopy and has the potential to be extended to other scanning transmission techniques and to characterize many emerging material systems.
引用
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页数:11
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