Relative assessment of the microstructure, properties and bioactivity of 3D-printed and rolled Ti6Al4V with micro-arc oxidation (MAO) and hydrothermal (HT) treatment

被引:1
作者
Zhang, Yingpeng [1 ]
Luo, Sisi [1 ]
Zhong, Yuan [1 ]
Wang, Qun [1 ]
Ramachandran, Chidambaram Seshadri [2 ]
机构
[1] Hunan Univ, Coll Mat Sci & Engn, Changsha 410082, Hunan, Peoples R China
[2] SUNY Stony Brook, Dept Mat Sci & Engn, New York, NY 11794 USA
来源
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T | 2023年 / 27卷
关键词
3D printing; Ti6Al4V; Micro-arc oxidation; Hydrothermal; Physical properties; Bioactivity; ENHANCED OSSEOINTEGRATION; TITANIUM; SURFACE;
D O I
10.1016/j.jmrt.2023.11.020
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The surface modification of 3D printed Ti6Al4V (3D-Ti64) and rolled Ti6Al4V (RO-Ti64) was carried out using optimized micro-arc oxidation (MAO) and hydrothermal (HT) treatment processes. The results showed that the 3D-Ti64 coating had a typical porous structure that was identical to the phase composition of the RO-Ti64 coating, and both exhibited super hydrophilic properties (contact angle of 0 degrees). It was found that the 3D-Ti64 coating (1.40 x 10-7A/cm2, 39.38 MPa) had greater corrosion current density and adhesion strength compared to the RO-Ti64 coating (0.76 x 10-7A/cm2, 33.69 MPa). In addition, the HAP crystals formed by 3D-Ti64 and RO-Ti64 coatings after being cultured in SBF were not significantly different, indicating that both coatings had comparable in vitro bioactivity. However, the 3D-printed porous Ti64 coating formed a porous structure only around the edges, while the central region had a flocculent structure with unfinished electrolytic oxidation. Moreover, it was found that more HAP crystals were formed in the edge region after HT treatment. In short, the MAO and HT treatment parameters optimized on rolled Ti alloys can be inherited for continued use on 3D-printed Ti alloy solids. However, more considerations may need to be made for the 3D printing of porous Ti alloys.
引用
收藏
页码:4805 / 4811
页数:7
相关论文
共 29 条
  • [1] Hydroxyapatite production on ultrafine-grained pure titanium by micro-arc oxidation and hydrothermal treatment
    Alsaran, A.
    Purcek, G.
    Hacisalihoglu, I.
    Vangolu, Y.
    Bayrak, O.
    Karaman, I.
    Celik, A.
    [J]. SURFACE & COATINGS TECHNOLOGY, 2011, 205 : S537 - S542
  • [2] Plasma sprayed fluoride and zinc doped hydroxyapatite coated titanium for load-bearing implants
    Bhattacharjee, Arjak
    Bandyopadhyay, Amit
    Bose, Susmita
    [J]. SURFACE & COATINGS TECHNOLOGY, 2022, 440
  • [3] Rapidly formation of the highly bioactive surface with hydroxyapatite crystals on the titania micro arc oxidation coating by microwave hydrothermal treatment
    Du, Qing
    Wei, Daqing
    Wang, Shaodong
    Cheng, Su
    Wang, Yaming
    Li, Baoqiang
    Jia, Dechang
    Zhou, Yu
    [J]. APPLIED SURFACE SCIENCE, 2019, 487 : 708 - 718
  • [4] The effect of applied voltages on the structure, apatite-inducing ability and antibacterial ability of micro arc oxidation coating formed on titanium surface
    Du, Qing
    Wei, Daqing
    Wang, Yaming
    Cheng, Su
    Liu, Shang
    Zhou, Yu
    Jia, Dechang
    [J]. BIOACTIVE MATERIALS, 2018, 3 (04) : 426 - 433
  • [5] Fast formation of a black inner α-Al2O3 layer doped with CuO on Al-Cu-Li alloy by soft sparking PEO process
    He, Xiaorui
    Feng, Tian
    Cheng, Yulin
    Hu, Panfeng
    Le, Zhengzhou
    Liu, Zihua
    Cheng, Yingliang
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2023, 106 (11) : 7019 - 7042
  • [6] Biocompatibility of micro/nano structures on the surface of Ti6Al4V and Ti-based bulk metallic glasses induced by femtosecond laser
    Huang, Hanxuan
    Zhang, Peilei
    Tang, Man
    Shen, Lei
    Yu, Zhishui
    Shi, Haichuan
    Tian, Yingtao
    [J]. BIOMATERIALS ADVANCES, 2022, 139
  • [7] Comparative Study on 3D Printed Ti6Al4V Scaffolds with Surface Modifications Using Hydrothermal Treatment and Microarc Oxidation to Enhance Osteogenic Activity
    Huang, Leizhen
    Cai, Bianyun
    Huang, Yong
    Wang, Jingcheng
    Zhu, Ce
    Shi, Kun
    Song, Yueming
    Feng, Ganjun
    Liu, Limin
    Zhang, Li
    [J]. ACS OMEGA, 2021, 6 (02): : 1465 - 1476
  • [8] Sol-Gel Derived Hydroxyapatite Coatings for Titanium Implants: A Review
    Jaafar, Alaa
    Hecker, Christine
    Arki, Pal
    Joseph, Yvonne
    [J]. BIOENGINEERING-BASEL, 2020, 7 (04): : 1 - 23
  • [9] Review on titanium and titanium based alloys as biomaterials for orthopaedic applications
    Kaur, Manmeet
    Singh, K.
    [J]. MATERIALS SCIENCE AND ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS, 2019, 102 : 844 - 862
  • [10] Enhanced Osseointegration of Hierarchical Micro/Nanotopographic Titanium Fabricated by Microarc Oxidation and Electrochemical Treatment
    Li, Guanglong
    Cao, Huiliang
    Zhang, Wenjie
    Ding, Xun
    Yang, Guangzheng
    Qiao, Yuqin
    Liu, Xuanyong
    Jiang, Xinquan
    [J]. ACS APPLIED MATERIALS & INTERFACES, 2016, 8 (06) : 3840 - 3852