HRTEM Characterization of an Age-Hardened Mg-Ca Binary Alloy

被引:0
作者
Unekawa, Mariko [1 ,2 ]
Terada, Yoshihiro [1 ]
机构
[1] Tokyo Inst Technol, Sch Mat & Chem Technol, Dept Mat Sci & Engn, Yokohama 2268502, Japan
[2] LIXIL Corp, Tokyo, Japan
关键词
magnesium-calcium alloy; Mg2Ca; aging; coherency; high-resolution transmission electron microscopy (HRTEM); PRECIPITATION;
D O I
10.2320/jinstmet.J2023002
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
A Mg-2.8 mass% Ca binary alloy was subjected to a homogenization treatment. The three-dimensional morphology and coherency of the parallel to the {1 ⠁010}& alpha; columnar plane of the & alpha;-Mg matrix. The coarsening Mg2Ca precipitate retained coherency with the & alpha;-Mg matrix for aging time of 3 h, which corresponded to the peak-aged condition. Furthermore, during the coarsening process, misfit dislocations were introduced on the planar surface of the precipitates, and the coherent interface became a semi-coherent interface for aging time of 100 h, which corresponded to the over-aged condition. The Mg2Ca precipitates evolved from a hexagonal plate-like morphology to a rectangular morphology and then to a polygonal morphology during aging treatment at 423 K. [doi:10.2320/jinstmet.J2023002]
引用
收藏
页码:231 / 234
页数:4
相关论文
共 12 条
[1]   Intermetallics in magnesium alloys [J].
Hort, N ;
Huang, YD ;
Kainer, KU .
ADVANCED ENGINEERING MATERIALS, 2006, 8 (04) :235-240
[2]   Enhanced precipitation hardening of Mg-Ca alloy by Al addition [J].
Jayaraj, J. ;
Mendis, C. L. ;
Ohkubo, T. ;
Oh-ishi, K. ;
Hono, K. .
SCRIPTA MATERIALIA, 2010, 63 (08) :831-834
[3]   C15-Al2Ca Precipitation in a Mg-Al-Ca Alloy [J].
Kashiwase, Sakiko ;
Unekawa, Mariko ;
Hisazawa, Hiromu ;
Terada, Yoshihiro .
MATERIALS TRANSACTIONS, 2020, 61 (02) :375-380
[4]   Three-Dimensional Morphology of C15-Al2Ca Precipitates in a Mg-Al-Ca Alloy [J].
Kashiwase, Sakiko ;
Unekawa, Mariko ;
Hisazawa, Hiromu ;
Terada, Yoshihiro .
MATERIALS TRANSACTIONS, 2019, 60 (09) :2048-2052
[5]   The 400 °C isothermal section of the Mg-Al-Ca system [J].
Kevorkov, D. ;
Medraj, M. ;
Li, Jian ;
Essadiqi, E. ;
Chartrand, P. .
INTERMETALLICS, 2010, 18 (08) :1498-1506
[6]  
Massalski T B., 1990, Binary Alloy Phase Diagrams
[7]   Precipitation and Hardening in Magnesium Alloys [J].
Nie, Jian-Feng .
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 2012, 43A (11) :3891-3939
[8]   TEM and 3DAP characterization of an age-hardened Mg-Ca-Zn alloy [J].
Oh, JC ;
Ohkubo, T ;
Mukai, T ;
Hono, K .
SCRIPTA MATERIALIA, 2005, 53 (06) :675-679
[9]   Age-hardening response of Mg-0.3 at.%Ca alloys with different Zn contents [J].
Oh-ishi, K. ;
Watanabe, R. ;
Mendis, C. L. ;
Hono, K. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 526 (1-2) :177-184
[10]   Precipitation strengthening of a Mg-Al-Ca-based AXJ530 die-cast alloy [J].
Suzuki, A. ;
Saddock, N. D. ;
Terbush, J. R. ;
Powell, B. R. ;
Jones, J. W. ;
Pollock, T. M. .
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 2008, 39A (03) :696-702