Characterization of Nanomaterials Using In Situ Liquid-Cell Transmission Electron Microscopy: A Review

被引：2
作者：
Chen, Yinci [1 ]
Yin, Kuibo [1 ,2 ,3 ]
Xu, Tao [1 ,2 ,3 ]
Guo, Hongxuan [1 ,2 ,3 ]
Sun, Litao [1 ,2 ]
机构：
[1] Southeast Univ, Sch Integrated Circuits, Wuxi 214000, Peoples R China
[2] Southeast Univ, SEU FEI Nanopico Ctr, Minist Educ, Key Lab MEMS, Nanjing 210096, Peoples R China
[3] Southeast Univ, Sch Elect Sci & Engn, Nanjing 210096, Peoples R China
来源：
ACS APPLIED NANO MATERIALS | 2023年 / 6卷 / 24期
基金：
中国国家自然科学基金;
关键词：
in situ liquid-phase characterization; in situ liquid-cell TEM; micro/nanofabrication; 2D window membrane materials; characterization of nanomaterialsin solution; image resolution; electron beam effects; LITHIUM-ION BATTERIES; WET-CELL; DIRECT VISUALIZATION; NANOCRYSTAL GROWTH; INTERPHASE FORMATION; LOCALIZED CORROSION; BEAM MANIPULATION; HIGH-QUALITY; GRAPHENE; TEM;
D O I：
10.1021/acsanm.3c03003
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
In the realm of nanocharacterization, a myriad of techniques have been engineered to facilitate in situ visualization of liquid samples through transmission electron microscopy (TEM). This advancement has opened avenues for real-time and dynamic inspection of both liquid samples and nanomaterials in solution. This Review introduces the methodologies employed in liquid-phase TEM characterization. It then delves into the architecture, fabrication, and applications of the liquid cells utilized in TEM, underscoring their significant role in nanomaterial characterization. It also highlights the impact of image resolution and electron beam damage on the development of liquid-cell TEM. Next, the fabrication processes of silicon nitride and graphene, which serve as window materials in liquid cells, are examined. This examination hints at the potential development of novel window materials, such as MoS2. Finally, future opportunities and challenges for liquid-cell TEM development are discussed. This Review provides a comprehensive exploration of liquid cells in the context of TEM characterization.
引用
收藏
页码：22545 / 22567
页数：23
相关论文
共 222 条
  • [1] Adiga V. P., 2016, US Patent, Patent No. [20160042912A1, 20160042912]
  • [2] Unravelling Kinetic and Thermodynamic Effects on the Growth of Gold Nanoplates by Liquid Transmission Electron Microscopy
    Alloyeau, Damien
    Dachraoui, Walid
    Javed, Yasir
    Belkahla, Hannen
    Wang, Guillaume
    Lecoq, Helene
    Ammar, Souad
    Ersen, Ovidiu
    Wisnet, Andreas
    Gazeau, Florence
    Ricolleau, Christian
    [J]. NANO LETTERS, 2015, 15 (04) : 2574 - 2581
  • [3] Ligand-Dependent Coalescence Behaviors of Gold Nanoparticles Studied by Multichamber Graphene Liquid Cell Transmission Electron Microscopy
    Bae, Yuna
    Lim, Kitaek
    Kim, Seulwoo
    Kang, Dohun
    Kim, Byung Hyo
    Kim, Joodeok
    Kang, Sungsu
    Jeon, Sungho
    Cho, JunBeom
    Lee, Won Bo
    Lee, Won Chul
    Park, Jungwon
    [J]. NANO LETTERS, 2020, 20 (12) : 8704 - 8710
  • [4] Nanoparticle movement: Plasmonic forces and physical constraints
    Batson, P. E.
    Reyes-Coronado, A.
    Barrera, R. G.
    Rivacoba, A.
    Echenique, P. M.
    Aizpurua, J.
    [J]. ULTRAMICROSCOPY, 2012, 123 : 50 - 58
  • [5] Plasmonic Nanobilliards: Controlling Nanoparticle Movement Using Forces Induced by Swift Electrons
    Batson, P. E.
    Reyes-Coronado, A.
    Barrera, R. G.
    Rivacoba, A.
    Echenique, P. M.
    Aizpurua, J.
    [J]. NANO LETTERS, 2011, 11 (08) : 3388 - 3393
  • [6] Real-time imaging of activation and degradation of carbon supported octahedral Pt-Ni alloy fuel cell catalysts at the nanoscale using in situ electrochemical liquid cell STEM
    Beermann, Vera
    Holtz, Megan E.
    Padgett, Elliot
    de Araujo, Jorge Ferreira
    Muller, David A.
    Strasser, Peter
    [J]. ENERGY & ENVIRONMENTAL SCIENCE, 2019, 12 (08) : 2476 - 2485
  • [7] In situ electrochemistry inside a TEM with controlled mass transport
    Beker, Anne France
    Sun, Hongyu
    Lemang, Mathilde
    van Omme, J. Tijn
    Spruit, Ronald G.
    Bremmer, Marien
    Basak, Shibabrata
    Garza, H. Hugo Perez
    [J]. NANOSCALE, 2020, 12 (43) : 22192 - 22201
  • [8] Controlling dissolution of PbTe nanoparticles in organic solvents during liquid cell transmission electron microscopy
    Bhattarai, Nabraj
    Woodall, Danielle L.
    Boercker, Janice E.
    Tischler, Joseph G.
    Brintlinger, Todd H.
    [J]. NANOSCALE, 2019, 11 (31) : 14573 - 14580
  • [9] Machine Learning Method Reveals Hidden Strong Metal-Support Interaction in Microscopy Datasets
    Blum, Thomas
    Graves, Jeffery
    Zachman, Michael J.
    Polo-Garzon, Felipe
    Wu, Zili
    Kannan, Ramakrishnan
    Pan, Xiaoqing
    Chi, Miaofang
    [J]. SMALL METHODS, 2021, 5 (05)
  • [10] Ultrahigh electron mobility in suspended graphene
    Bolotin, K. I.
    Sikes, K. J.
    Jiang, Z.
    Klima, M.
    Fudenberg, G.
    Hone, J.
    Kim, P.
    Stormer, H. L.
    [J]. SOLID STATE COMMUNICATIONS, 2008, 146 (9-10) : 351 - 355
12345678910