Analytical Capabilities of the Determination of Carbohydrates by Chromatographic and Electrophoretic Methods

被引：2

作者：

Kartsova, L. A. ^{[1
]}

Maliushevska, A. V. ^{[1
]}

Kolobova, E. A. ^{[1
,2
]}

机构：

[1] St Petersburg State Univ, St Petersburg 198504, Russia

[2] EMERCOM Russia, Nikiforov Russian Ctr Emergency & Radiat Med, St Petersburg 194044, Russia

来源：

JOURNAL OF ANALYTICAL CHEMISTRY | 2023年 / 78卷 / 02期

基金：

俄罗斯科学基金会;

关键词：

capillary electrophoresis; high performance liquid chromatography; neutral carbohydrates; derivatization; indirect detection; ligand-exchange capillary electrophoresis; CAPILLARY-ZONE-ELECTROPHORESIS; SOLID-PHASE EXTRACTION; PRESSURIZED LIQUID EXTRACTION; PULSED AMPEROMETRIC DETECTION; INDIRECT UV DETECTION; AMINO-ACIDS; MONOSACCHARIDE COMPOSITION; 2-AMINOBENZOIC ACID; INORGANIC ANIONS; ANTHRANILIC ACID;

D O I：

10.1134/S1061934823020041

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The review discusses the advantages and limitations of chromatographic and electrophoretic approaches to the determination of neutral carbohydrates in various samples with complex matrices, the possibility of implementing a variety of liquid chromatography and capillary electrophoresis modes (in zone and micellar versions), and their combinations with various derivatization, detection, and sample preparation techniques. Conditions for the indirect detection of sugars upon the introduction of various absorbing additives into a mobile phase or supporting electrolyte, ligand-exchange capillary electrophoresis, and intracapillary complexation and the determination of carbohydrates by anion-exchange and hydrophilic chromatography are discussed.

引用

页码：144 / 161

页数：18

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