Iron oxide nanoparticles produced by the laser ablation technique and analyzed by x-ray photoelectron spectroscopy

被引:0
作者
Gonzalez, E. David [1 ]
Botero, M. A. [1 ]
Ospina, R. [2 ]
机构
[1] Univ Ind Santander, Escuela Ingn Elect Elect & telecomunicac E3T, Grp Invest Sistemas Energia Electr GISEL, Bucaramanga 680002, Santander, Colombia
[2] Univ Ind Santander, Ctr Invest Cient & Tecnol Mat & Nanociencias CMN, Piedecuesta 681011, Santander, Colombia
来源
SURFACE SCIENCE SPECTRA | 2024年 / 31卷 / 01期
关键词
Iron oxide; XPS; Nanoparticles; Magnetic nanoparticles; PLD; ALPHA-FE2O3; NANOPARTICLES; XPS ANALYSIS; PRECIPITATION; FE3O4;
D O I
10.1116/6.0002839
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
The study of iron nanoparticles is one of the most researched areas in recent times due to the potential applications they have and because the study of iron by XPS is one of the most debated elements. In this work, we provide investigation data of iron oxide nanoparticles produced using the laser ablation technique, which were characterized using x-ray photoelectron spectroscopy. Survey spectra, C 1s, O 1s, and Fe 2p core levels spectra were acquired. Results showed the presence of Fe+3 and Fe+2 elements that constitute hematite and magnetite with differences in their concentrations depending on the fitting method. In addition, the presence of adventitious carbon and carbon from impurities was detected.
引用
收藏
页数:7
相关论文
共 19 条
[1]  
Barcena C., 2009, Nanoscale Magnetic Materials and Applications, V167, p591.
[2]   MAGNETIC-STRUCTURE OF NONSTOICHIOMETRIC FERROUS OXIDE [J].
BATTLE, PD ;
CHEETHAM, AK .
JOURNAL OF PHYSICS C-SOLID STATE PHYSICS, 1979, 12 (02) :337-345
[3]   Accessing the robustness of adventitious carbon for charge referencing (correction) purposes in XPS analysis: Insights from a multi-user facility data review [J].
Biesinger, Mark C. .
APPLIED SURFACE SCIENCE, 2022, 597
[4]   Resolving surface chemical states in XPS analysis of first row transition metals, oxides and hydroxides: Cr, Mn, Fe, Co and Ni [J].
Biesinger, Mark C. ;
Payne, Brad P. ;
Grosvenor, Andrew P. ;
Lau, Leo W. M. ;
Gerson, Andrea R. ;
Smart, Roger St. C. .
APPLIED SURFACE SCIENCE, 2011, 257 (07) :2717-2730
[5]   Investigation of multiplet splitting of Fe 2p XPS spectra and bonding in iron compounds [J].
Grosvenor, AP ;
Kobe, BA ;
Biesinger, MC ;
McIntyre, NS .
SURFACE AND INTERFACE ANALYSIS, 2004, 36 (12) :1564-1574
[6]   CALCULATION OF MULTIPLET STRUCTURE OF CORE P-VACANCY LEVELS .2. [J].
GUPTA, RP ;
SEN, SK .
PHYSICAL REVIEW B, 1975, 12 (01) :15-19
[7]   Synthesis, photoluminescence and Magnetic properties of iron oxide (α-Fe2O3) nanoparticles through precipitation or hydrothermal methods [J].
Lassoued, Abdelmajid ;
Lassoued, Mohamed Saber ;
Dkhil, Brahim ;
Ammar, Salah ;
Gadri, Abdellatif .
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, 2018, 101 :212-219
[8]   Synthesis, structural, morphological, optical and magnetic characterization of iron oxide (α-Fe2O3) nanoparticles by precipitation method: Effect of varying the nature of precursor [J].
Lassoued, Abdelmajid ;
Lassoued, Mohamed Saber ;
Dkhil, Brahim ;
Ammar, Salah ;
Gadri, Abdellatif .
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, 2018, 97 :328-334
[9]   Structure of magnetite (Fe3O4) above the Curie temperature: a cation ordering study [J].
Levy, Davide ;
Giustetto, Roberto ;
Hoser, Andreas .
PHYSICS AND CHEMISTRY OF MINERALS, 2012, 39 (02) :169-176
[10]   A consistent method for quantitative XPS peak analysis of thin oxide films on clean polycrystalline iron surfaces [J].
Lin, TC ;
Seshadri, G ;
Kelber, JA .
APPLIED SURFACE SCIENCE, 1997, 119 (1-2) :83-92