Application of Ti-MOF-UR as a new porous catalyst for the preparation of pyrazolo[3,4-b]quinoline and pyrazolo[4,3-e]pyridines

被引：18

作者：

Torkashvand, Zahra ^{[1
]}

Sepehrmansourie, Hassan ^{[1
]}

Zolfigol, Mohammad Ali ^{[1
]}

As'Habi, Mohammad Ali ^{[2
]}

机构：

[1] Bu Ali Sina Univ, Fac Chem, Dept Organ Chem, Hamadan 6517838683, Iran

[2] Shahid Beheshti Univ, Med Plant & Drugs Res Inst, Dept Phytochem, Tehran 1983963113, Iran

来源：

MOLECULAR CATALYSIS | 2023年 / 541卷

基金：

美国国家科学基金会;

关键词：

H -bond catalyst; Metal -organic frameworks (MOFs); MIL-125(Ti)-NH 2; MIL-125(Ti)-NH2; Pyrazolo[3; 4-b]quinolines; Pyrazolo[4; 3-e]pyridines; METAL-ORGANIC FRAMEWORKS; 3-COMPONENT SYNTHESIS; BIOLOGICAL EVALUATION; EFFICIENT; DESIGN; ORGANOCATALYST; DERIVATIVES; STORAGE; SIZE;

D O I：

10.1016/j.mcat.2023.113107

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A new H-bond Ti-MOF-based catalyst via the post-modification method of metal-organic frameworks (MOFs) was synthesized. The catalytic role of Ti-MOF-UR is based on hydrogen-bond interaction. Ti-MOF-UR was used to synthesize pyrazolo[3,4-b]quinolines and pyrazolo[4,3-e]pyridines that contain the biological nuclei of pyrazole, henna and coumarin. The structure of the synthesized catalyst as well as the pyrazolo[3,4-b]quinoline and pyrazolo[4,3-e]pyridine derivatives were approved by using various instrumental techniques such as melting point, FT-IR, 1H NMR, 13C NMR and HR-MS techniques.

引用

页数：12

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