A simple, rapid and sensitive analytical method for the determination of hydroxylamine in water samples using modified glassy carbon electrode

被引：2
|
作者：
Basande, Ashkan [1 ]
Beitollahi, Hadi [2 ]
机构：
[1] Grad Univ Adv Technol, Dept Chem, Kerman, Iran
[2] Grad Univ Adv Technol, Inst Sci & High Technol & Environm Sci, Environm Dept, Kerman, Iran
来源：
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS | 2023年 / 34卷 / 07期
关键词：
ELECTROCHEMICAL DETERMINATION; VOLTAMMETRIC DETERMINATION; ELECTROCATALYTIC OXIDATION; NANOPARTICLES; SPHERES; SENSOR; OXIDE; FABRICATION; HYDRAZINE; COMPOSITE;
D O I：
10.1007/s10854-023-09891-w
中图分类号：
TM [电工技术]; TN [电子技术、通信技术];
学科分类号：
0808 ; 0809 ;
摘要：
The current work was undertaken to modify glassy carbon electrode (GCE) surface with nitrogen-doped hollow carbon spheres (N-HCSs) for determination of hydroxylamine. Differential pulse voltammetry (DPV), cyclic voltammetry (CV) and chronoamperometry (CA) were recruited for electrochemical analysis, the results of which revealed the admirable performance of N-HCSs/GCE for the hydroxylamine determination, with broad linear dynamic range from 10.0 to 100.0 mu M, and narrow limit of detection (LOD) of 3.0 mu M. Moreover, N-HCSs/GCE had successful applicability for sensing the hydroxylamine found in real water specimens.
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页数：11
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