Hydrothermal oxidation of titanium nitride coating for enhanced corrosion resistance in fluoride-containing acidic solution

被引：2

作者：

Ren, Jian ^{[1
]}

Xu, Lingli ^{[1
]}

Luo, Junjie ^{[1
]}

Li, Zhihan ^{[1
]}

Li, Boxuan ^{[2
]}

Shi, Xingling ^{[1
]}

Xu, Lin ^{[3
]}

Bang, Le Thi ^{[4
]}

Fu, Qingshan ^{[5
]}

机构：

[1] Jiangsu Univ Sci & Technol, Sch Mat Sci & Engn, Zhenjiang 212100, Peoples R China

[2] Rutgers State Univ, Dept Chem & Chem Biol, Piscataway, NJ 08854 USA

[3] Jiangsu Univ, Inst Intelligent Flexible Mechatron, Zhenjiang 212013, Peoples R China

[4] Hanoi Univ Sci & Technol, Sch Mat Sci & Engn, Hanoi 10000, Vietnam

[5] Sichuan Univ Sci & Engn, Mat Corros & Protect Key Lab Sichuan Prov, Chengdu 643000, Peoples R China

来源：

MATERIALS LETTERS | 2023年 / 335卷

关键词：

Titanium nitride; Surface; Oxidation; Hydrothermal; Fluoride; Corrosion;

D O I：

10.1016/j.matlet.2022.133790

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

To improve the corrosion resistance of titanium nitride (TiN) coating in acidic solution containing fluoride ions (F-), surface hydrothermal oxidation was conducted. Pure water was used as the medium and at temperatures as low as 200-250 degrees C, a thin, uniform and dense titanium oxide (TiO2) nanolayer composed of well-crystallized anatase nanoparticles was fabricated. The TiO2 layer was grown in situ, and its (004) planes aligned well with the (1 1 1) planes of underlying TiN; the transition zone was only a few atomic layers thick. Hydrothermal oxidation improved the chemical stability and decreased the corrosion rate of TiN coating in 0.5 mol/L sulfuric acid solution containing 0.05 wt% F-. When fabricated at 250 degrees C, the TiO2 layer remained intact after immersion test, providing good protection for the underlying TiN.

引用

页数：4

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