Hydrothermal oxidation of titanium nitride coating for enhanced corrosion resistance in fluoride-containing acidic solution

被引：4
作者：
Ren, Jian [1 ]
Xu, Lingli [1 ]
Luo, Junjie [1 ]
Li, Zhihan [1 ]
Li, Boxuan [2 ]
Shi, Xingling [1 ]
Xu, Lin [3 ]
Bang, Le Thi [4 ]
Fu, Qingshan [5 ]
机构：
[1] Jiangsu Univ Sci & Technol, Sch Mat Sci & Engn, Zhenjiang 212100, Peoples R China
[2] Rutgers State Univ, Dept Chem & Chem Biol, Piscataway, NJ 08854 USA
[3] Jiangsu Univ, Inst Intelligent Flexible Mechatron, Zhenjiang 212013, Peoples R China
[4] Hanoi Univ Sci & Technol, Sch Mat Sci & Engn, Hanoi 10000, Vietnam
[5] Sichuan Univ Sci & Engn, Mat Corros & Protect Key Lab Sichuan Prov, Chengdu 643000, Peoples R China
来源：
MATERIALS LETTERS | 2023年 / 335卷
关键词：
Titanium nitride; Surface; Oxidation; Hydrothermal; Fluoride; Corrosion;
D O I：
10.1016/j.matlet.2022.133790
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
To improve the corrosion resistance of titanium nitride (TiN) coating in acidic solution containing fluoride ions (F-), surface hydrothermal oxidation was conducted. Pure water was used as the medium and at temperatures as low as 200-250 degrees C, a thin, uniform and dense titanium oxide (TiO2) nanolayer composed of well-crystallized anatase nanoparticles was fabricated. The TiO2 layer was grown in situ, and its (004) planes aligned well with the (1 1 1) planes of underlying TiN; the transition zone was only a few atomic layers thick. Hydrothermal oxidation improved the chemical stability and decreased the corrosion rate of TiN coating in 0.5 mol/L sulfuric acid solution containing 0.05 wt% F-. When fabricated at 250 degrees C, the TiO2 layer remained intact after immersion test, providing good protection for the underlying TiN.
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页数：4
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