Synthesis and Characterization of a Soluble Hemihexaphyrazine Derivative

被引：1
作者：
Kibireva, Yana E. [1 ,2 ]
Islyaikin, Mikhail K. [1 ,2 ]
Rodriguez-Morgade, M. Salome [3 ]
Torres, Tomas [1 ,3 ]
机构：
[1] Ivanovo State Univ Chem & Technol, Res Inst Macroheterocycles, IRLoN, Ivanovo 153000, Russia
[2] Russian Acad Sci, GA Krestov Inst Solut Chem, Ivanovo 153045, Russia
[3] Univ Autonoma Madrid, Dept Organ Chem, Madrid 28049, Spain
来源：
MACROHETEROCYCLES | 2023年 / 16卷 / 01期
关键词：
Expanded azaporphyrin; hemihexaphyrazine; 1; 3; 4-thiadiazole; hexaphyrin; HEMIPORPHYRAZINE; PHTHALOCYANINES;
D O I：
10.6060/mhc234968i
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The symmetrically substituted hexakis(n-hexyl)hemihexaphyrazine was synthesized by condensation of 3,6 -bis(n-hexyl)phthalonitrile and 2,5-diamino-1,3,4-thiadiazole in the presence of sodium pentanolate. The macro cycle was characterized by MALDI-TOF mass spectrometry, as well as IR, 1H and 13C NMR, UV-Vis absorption and fluores-cence spectroscopies.
引用
收藏
页码：19 / 23
页数：5
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