Fe/ZSM-5-Catalyzed-Synthesis of 1,4-Dihydropyridines under Ultrasound Irradiation and Their Antioxidant Activities (Fe/ZSM-5-Pemangkin-Sintesis 1,4-Dihidropiridin di Bawah Sinaran Ultrabunyi dan Aktiviti Antioksidannya)

被引：2
作者：
Sutarni, Yayan Dwi [1 ]
Purwono, Bambang [1 ]
Kunarti, Eko Sri [1 ]
Mardjan, Muhammad Idham Darussalam [1 ]
机构：
[1] Univ Gadjah Mada, Fac Math & Nat Sci, Dept Chem, Yogyakarta 55281, Indonesia
来源：
SAINS MALAYSIANA | 2023年 / 52卷 / 04期
关键词：
Antioxidant assay; Fe; ZSM-5; catalyst; ultrasound-assisted-multicomponent reaction; 1; 4-dihydropyridines; ONE-POT SYNTHESIS; HANTZSCH REACTION; IONIC LIQUID; GREEN; EFFICIENT; CATALYST; CONVERSION; CHEMISTRY; ZEOLITES; H-ZSM-5;
D O I：
10.17576/jsm-2023-5204-12
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
A small library of 1,4-dihydropyridines have been synthesized from ethyl acetoacetate, ammonium acetate and various aldehydes via Hantzsch multicomponent reaction in the presence of Fe/ZSM-5 catalyst under ultrasound irradiation for 90 min. 1,4-Dihydropyridine derivatives were obtained in 64-86% yields and the heterogeneous Fe/ZSM-5 catalyst can be employed for four reaction cycles without losing the catalytic activity. All products were evaluated for their antioxidant activities using the DPPH method and compound 4g was found to be an effective antioxidant agent with DPPH activity of 83.5%.
引用
收藏
页码：1189 / 1202
页数：14
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