Effect of heat treatments on Inconel 625 fabricated by wire and arc additive manufacturing: an in situ synchrotron X-ray diffraction analysis

被引:32
作者
Rodrigues, Tiago A. [1 ]
Farias, Francisco Werley Cipriano [1 ]
Avila, Julian A. [2 ]
Maawad, Emad [3 ]
Schell, Norbert [3 ]
Santos, Telmo G. [1 ]
Oliveira, J. P. [1 ,4 ,5 ,6 ]
机构
[1] Univ NOVA Lisboa Caparica, NOVA Sch Sci & Technol, Dept Mech & Ind Engn, UNIDEMI, Caparica, Portugal
[2] Univ Politecn Cataluna, Barcelona Sch Engn ETSEIB, Dept Strength Mat & Struct Engn, Barcelona, Spain
[3] Inst Mat Phys, Helmholtz Zentrum Hereon, Geesthacht, Germany
[4] Univ NOVA Lisboa, Dept Mat Sci, NOVA Sch Sci & Technol, CENIMAT-I3N, Caparica, Portugal
[5] Univ NOVA Lisboa, NOVA Sch Sci & Technol, Dept Mech & Ind Engn, UNIDEMI, P-2829516 Caparica, Portugal
[6] Univ NOVA Lisboa, NOVA Sch Sci & Technol, Dept Mat Sci, CENIMAT-I3N, P-2829516 Caparica, Portugal
关键词
Synchrotron radiation; nickel alloys; hardness test; isothermal heat treatments; wire and arc additive manufacturing; MECHANICAL-PROPERTIES; DELTA-PHASE; MICROSTRUCTURE; TEMPERATURE;
D O I
10.1080/13621718.2023.2187927
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The effect of heat treatments on wire and arc additively manufactured Inconel 625 parts was investigated using in situ synchrotron X-ray diffraction and hardness testing. As-built samples revealed the presence of a gamma-matrix with precipitation of gamma ', gamma '' and MC carbides. When heat treated at 750 degrees C for 4 h, gamma '' phase precipitated increasing the hardness by 5%. In situ X-ray observations revealed that heat treating at 870 degrees C for 1 h resulted in delta-phase precipitation. Two different second-stage temperatures were tested (1050 degrees C and 1150 degrees C), which dissolved the delta-phase while MC carbides formed upon cooling. The second stage at 1150 degrees C had a higher deleterious effect than the one performed at 1050 degrees C due to extensive grain growth.
引用
收藏
页码:534 / 539
页数:6
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