Effects of post-processing curing parameters and gamma irradiation on the mechanical properties of medical graded vat photopolymerization parts

被引:2
作者
Daoset, Natthawut [1 ]
Inglam, Samroeng [2 ]
Wanchat, Sujin [1 ,3 ]
Chantarapanich, Nattapon [1 ,3 ]
机构
[1] Kasetsart Univ, Fac Engn Sriracha, Dept Mech Engn, Chon Buri, Thailand
[2] Thammasat Univ, Fac Dent, Pathum Thani, Thailand
[3] Kasetsart Univ, Digital Ind Design & Mfg Res Unit, Chon Buri, Thailand
关键词
Mechanical properties; Gamma irradiation; Medical grade; Post-curing; Vat photopolymerization; STEREOLITHOGRAPHY; 3D; RECONSTRUCTION;
D O I
10.1108/RPJ-07-2023-0226
中图分类号
TH [机械、仪表工业];
学科分类号
0802 ;
摘要
PurposeThis paper aims to investigate the influence of post-curing temperature, post-curing time and gamma ray irradiation dose upon the tensile and compressive mechanical properties of the medical graded vat photopolymerization parts.Design/methodology/approachMedical graded vat photopolymerization specimens, made from photopolymer resin, were fabricated using bottom-up vat photopolymerization machine. Tensile and compressive tests were conducted to assess the mechanical properties. The specimens were categorized into uncured and post-curing groups. Temperature post-processing and/or gamma irradiation exposure were for post-curing specimens. The post-curing parameters considered included temperature levels of 50 degrees C, 60 degrees C and 70 degrees C, with 1, 2, 3 and 4 h periods. For the gamma irradiation, the exposure doses were 25, 50, 75 and 100 kGy.FindingsPost-curing improved the mechanical properties of medical graded vat photopolymerization parts for both tensile and compressive specimens. Post-curing temperature greater than 50 degrees C or a prolonged post-curing period of more than 1 h made insignificant changes or deterioration in mechanical properties. The optimal post-curing condition was therefore a 50 degrees C post-curing temperature with 1 h post-curing time. Exposure to gamma ray improved the compressive mechanical properties, but deteriorated tensile mechanical properties. Higher gamma irradiation doses could decrease the mechanical properties and also make the part more brittle, especially for doses more than 25 kGy.Originality/valueThe obtained results would be beneficial to the medical device manufacturer who fabricated the invasive temporary contact personalized surgical instruments by vat photopolymerization technique. In addition, it also raised awareness in excessive gamma sterilization in the medical graded vat photopolymerization parts.
引用
收藏
页码:475 / 489
页数:15
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