Synthesis and Crystal Structure of N-(1-Phenyl-3methyl-4-benzal-pyrazolone-5)-furoic Hydrazide

被引：0

作者：

LIU Langa JI YaLia JIA DianZenga YU KaiBeib aInstitute of Applied Chemistry Xinjiang University Urumqi China bChengdu Institute of Organic Chemistry The Chinese Academy of Sciences Chengdu China ^{[830046
,610012
]}

机构：

来源：

结构化学 | 2003年 / 05期

关键词：

synthesis; crystal structure; furoic hydrazide; pyrazolone;

D O I：

10.14102/j.cnki.0254-5861.2003.05.015

中图分类号：

O626 [杂环化合物];

学科分类号：

070303 ; 081704 ;

摘要：

N-(1-Phenyl-3-methyl-4-benzal-pyrazolone-5)-furoic hydrazide (PMBP-FUH, C22H18N4O3, CCDC No: 188946) has been synthesized and characterized by IR spectrum, 1H NMR and single-crystal X-ray diffraction. The crystal is of orthorhombic, space group Pbca with a = 11.870(2), b = 15.951(3), c = 19.674(3) ? V = 3725.0(11) ?, Mr = 386.40, Z = 8, Dc = 1.378 g/cm3, F(000) = 1616, R = 0.0455 and wR = 0.0809. The inter- or intramolecular hydrogen bonds result in the formation of three-dimensional network structure.

引用

页码：569 / 573

页数：5