Synthesis and Crystal Structure of (E)-N,N′- dicyclohexyl-1-(3-(3,4-dihydroxyphenyl)acryloyl)urea

被引：0

作者：

蒙法艳 ^{[1
]}

李美娟 ^{[1
]}

谢娴娴 ^{[1
]}

林翠梧 ^{[1
]}

机构：

[1] College of Chemistry and Chemical Engineering, Guangxi University

来源：

结构化学 | 2012年 / 31卷 / 09期

基金：

中国国家自然科学基金;

关键词：

caffeic acid; crystal structure; synthesis;

D O I：

10.14102/j.cnki.0254-5861.2012.09.008

中图分类号：

O625 [芳香族化合物];

学科分类号：

070303 ; 081704 ;

摘要：

The title compound, (E)-N,N′-dicyclohexyl-1-(3-(3,4-dihydroxyphenyl)acryloyl)- urea (DDA), has been synthesized and characterized by FT-IR and 1H-NMR spectroscopy, ESI- MS, and X-ray single-crystal diffraction. Its crystallizes in monoclinic, space group C2/c with a = 20.483(12), b = 11.153(6), c = 21.134(12) , β = 117.098(7), V = 4298(4) 3, Z = 8, F(000) = 1664, Dc = 1.195 Mg/m3, Mr = 386.48, μ= 0.082 mm-1, the final R = 0.0474 and wR = 0.1370 for 4853 observed reflections with I > 2σ(I).

引用

页码：1281 / 1286

页数：6

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