Synthesis and Characterization of (4R,5R)-1,3-dioxolance-4,5-bis(2-pyridineacrboxylic acid)

被引：0

作者：

姜艳 ^{[1
,2
]}

卜云飞 ^{[2
]}

张致慧 ^{[2
]}

王乐勇 ^{[1
]}

孙小强 ^{[2
]}

机构：

[1] Key Laboratory of Mesoscopic Chemistry of Education, School of Chemistry and Chemical Engineering, Nanjing University

[2] Jiangsu Provincial Key Laboratory of Fine Petrochemical Engineering, Changzhou University

来源：

结构化学 | 2011年 / 30卷 / 09期

关键词：

pyridinecarboxylic acid derivatives; crystal structure; hydrogen bond;

D O I：

10.14102/j.cnki.0254-5861.2011.09.004

中图分类号：

O621.2 [有机化合物性质];

学科分类号：

070303 ; 081704 ;

摘要：

The title compound, (4R,5R)-1,3-dioxolance-4,5-bis(2-pyridineacrboxylic acid), has been synthesized and characterized by single-crystal X-ray diffraction, IR, NMR, and MS analyses. Crystal structure of the title compound was grown from ETOH by slow diffusion at room temperature. The title compound crystallizes in monoclinic, space group C2 with a = 17.805(3), b = 11.459(3), c = 11.1656(17) , β = 113.066(4)°, V = 2095.9(6) 3, Z = 4, F(000) = 880, Dc = 1.332 Mg/m-3, C23H20N2O6, Mr = 420.41 and μ = 0.10 mm-1

引用

页码：1221 / 1224

页数：4