Synthesis of Polycrystalline Yb:Gd3Ga5O12 Nanopowders by Homogeneous Precipitation Method

被引:0
作者
黄德馨 [1 ,2 ]
刘景和 [1 ]
机构
[1] Department of Materials Science and Engineering,Changchun University of Science and Technology
[2] Department of Materials Science and Engineering,Jilin Architectural and Civil Engineering Institute
关键词
Yb:Gd3Ga5O12; polycrystalline; homogeneous precipitation; nanopowders;
D O I
暂无
中图分类号
TF123 [粉末的制造方法];
学科分类号
080502 ;
摘要
The Ytterbium doped gadolinium gallium garnet [Yb3+:Gd3Ga5O12, Yb:GGG] precursor powders were synthesized via homogeneous precipitation method using Yb2O3, Ga2O3, Gd2O3 and ammonium bicarbonate [NH4HCO3] as precipitator, and ammonium sulfate [(NH4)2SO4] as additive. The evolution of phase composition and micro-structure of the powders were characterized by TG- DTA, XRD, IR, and TEM. The results indicate that all precursor powders completely transform to Yb:GGG phase by calcining at 900 ℃ for 8 h, the resultant powders are well dispersed and have smaller particle size approximately 80 nm owing to the electrostatic effect.
引用
收藏
页码:123 / 126
页数:4
相关论文
共 10 条
[1]   微乳液法制备纳米球形YAG:Ce3+荧光粉及其发光性能(英文) [J].
郭瑞 ;
曾人杰 ;
吴音 ;
王婷 ;
黄勇 .
硅酸盐学报, 2008, (03) :352-357
[2]  
Influence of Ga2O3 on the Spectroscopic and Lasing Properties of Yb3+-doped Fluorophosphate Glasses[J]. 徐时清.Journal of Wuhan University of Technology(Materials Science Edition). 2007(S1)
[3]   Effect of Heat Treatment on Crystallization of Nd:YAG Ceramics [J].
张华山 ;
苏春辉 .
Journal of Wuhan University of Technology(Materials Science Edition), 2007, (02) :333-336
[4]   掺杂YAG和GGG激光晶体热导率研究 [J].
王保松 ;
江海河 ;
贾先德 ;
张庆礼 ;
孙敦陆 ;
殷绍唐 .
激光技术, 2007, (02) :141-143
[5]   均相沉淀法制备Nd∶YAG透明激光陶瓷材料研究 [J].
宋琼 ;
苏春辉 ;
张洪波 ;
邵晶 ;
朱晓薇 .
激光与红外, 2006, (01) :44-46
[6]   提拉法生长钆镓石榴石(GGG)晶体 [J].
陶德节 ;
邾根祥 ;
闫如顺 ;
刘福云 ;
郭行安 ;
殷绍唐 .
量子电子学报, 2003, (05) :550-552
[7]  
Study on crystal growth of large size Nd 3+ :Gd 3 Ga 5 O 12 (Nd 3+ :GGG) by Czochralski method[J] . Z. Jia,X. Tao,C. Dong,X. Cheng,W. Zhang,F. Xu,M. Jiang.Journal of Crystal Growth . 2006 (2)
[8]  
Yb 3+ -doped Gd 3 Ga 5 O 12 garnet single crystals grown by the micro-pulling down technique for laser application. Part I: Spectroscopic properties and assignment of energy levels[J] . Y. Guyot,H. Canibano,C. Goutaudier,A. Novoselov,A. Yoshikawa,T. Fukuda,G. Boulon.Optical Materials . 2005 (11)
[9]   Processing materials with microwave energy [J].
Clark, DE ;
Folz, DC ;
West, JK .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2000, 287 (02) :153-158
[10]  
Precipitation and calcination processes for yttrium aluminum garnet precursors synthesized by the urea method. Naoya Matsushita, Noriyoshi Tsuchiya, Katsuto Nakatsuka. Journal of the American Ceramic Society . 1999