Synthesis and Crystal Structure of 2(1-Phenyl-3-methyl-5-chloro-1H-pyrazol- 4-yl)-3-(1-naphthoylamido)-4-thiazolidinone

被引：2

作者：

LI Minga b c WEN LiRongb JING ShuXiab ZHAO GuiLongb YANG HuaZhenga a Institute of Elementoorganic Chemistry Nankai University Tianjin China b College of Chemistry and Molecular Engineering Qingdao University of Science and Technology Qingdao China c State Key Laboratory of Applied Organic Chemistry Lanzhou University Lanzhou China ^{[300071
,266042
,730000
]}

机构：

来源：

结构化学 | 2004年 / 04期

关键词：

pyrazole; 4-thiazolidinone; crystal structure; synthesis;

D O I：

10.14102/j.cnki.0254-5861.2004.04.004

中图分类号：

O621 [有机化学一般性问题];

学科分类号：

070303 ; 081704 ;

摘要：

The crystal structure of 2(1-phenyl-3-methyl-5-chloro-1H-pyrazol-4-yl)-3-(1- naphthoylamido)-4-thiazolidinone (C24H19ClN4O2S, Mr = 462.94) has been determined by single- crystal X-ray diffraction method. The crystal belongs to monoclinic, space group P21/c with a = 11.623(5), b = 11.579(5), c = 16.619(7) ? b = 90.112(8), V = 2237(2) 3, Z = 4, Dc = 1.375 g/cm3, m = 0.294 mm-1, F(000) = 960, R = 0.0492 and wR = 0.0768 for 3932 unique reflections with 1897 observed ones (I > 2s(I)). X-ray analysis reveals that there exist both intra-and intermolecular hydrogen bonds in the crystal lattice.

引用

页码：366 / 370+352 +352

页数：6