An efficient synthesis of bis(indolyl)methanes and N,N'-alkylidene bisamides by Silzic under solvent free conditions

被引:0
作者
Hanan A.Soliman [1 ]
Ahmed Y.Mubarak [2 ]
Saad S.Elmorsy [2 ]
机构
[1] Photochemistry Department,National Research Centre
[2] Chemistry Department,Faculty of Science,Mansoura University
关键词
Bis(indolyl)methanes; N; N’-alkylidenebisamides; Acetamide; Mild conditions; Silzic;
D O I
暂无
中图分类号
O621.3 [有机合成化学];
学科分类号
070303 ; 081704 ;
摘要
An operationally simple and green method for the synthesis of a wide range of bis(indolyl)methanes,and N,N’-alkylidene bisamides under mild conditions,with excellent yields using Silzic,has been developed.This improved method furnishes in good yields bis(indolyl)methanes derivatives starting from indole and aldehydes,or ketones,and N,N’-alkylidene bisamides derivatives starting from acetamide and aldehydes.The catalytic system was reused up to three times with the same efficiency.
引用
收藏
页码:353 / 356
页数:4
相关论文
共 22 条
  • [1] Efficient and Eco-friendly Process for the Synthesis of Bi(indolyl)methanes Catalyzed by Sodium Hydrogensulfate Monohydrate in Ionic Liquid n-Butylpyridinium Tetrafluoroborate[J]. Li Ping ZHANG, Yi Qun LI*, Mei Yun ZHOU Department of Chemistry, Jinan University, Guangzhou 510632.Chinese Chemical Letters. 2006(06)
  • [2] A new and facile tetrachlorosilane-promoted one-pot condensation for the synthesis of a novel series of tetracyclic 1,5-thiazepines[J] . Tamer K. Khatab,Khairy A.M. El-Bayouki,Wahid M. Basyouni.Tetrahedron Letters . 2014 (44)
  • [3] Tandem synthesis of N , N ′-alkylidenebisamides promoted by nano-SnCl 4 .SiO 2[J] . BIBI FATEMEH MIRJALILI,MOHAMMAD ALI MIRHOSEINI.Journal of Chemical Sciences . 2013 (6)
  • [4] Silicon-mediated highly efficient synthesis of 1,8-dioxo-octahydroxanthenes and their transformation to novel functionalized pyrano-tetrazolo[1,5- a] azepine derivatives[J] . Hanan A. Soliman,Tarek A. Salama.Chinese Chemical Letters . 2013 (5)
  • [5] One-pot preparation of N , N ′-alkylidene bisamide derivatives catalyzed by silica supported polyphosphoric acid (SiO 2 -PPA)[J] . Mohammad Reza Mohammad Shafiee.Journal of Saudi Chemical Society . 2011
  • [6] A practical and efficient synthesis of bis(indolyl)methanes in water, and synthesis of di-, tri-, and tetra(bis-indolyl)methanes under thermal conditions catalyzed by oxalic acid dihydrate[J] . Ramin Ghorbani-Vaghei,Hojat Veisi,Hassan Keypour,Ahmad Ali Dehghani-Firouzabadi.Molecular Diversity . 2010 (1)
  • [7] Synthesis of Bis(indolyl)methanes Using Recyclable PEG-Supported Sulfonic Acid as Catalyst
    Shou-Ri Sheng
    Qiu-Ying Wang
    Yan Ding
    Xiao-Ling Liu
    Ming-Zhong Cai
    [J]. Catalysis Letters, 2009, 128 : 418 - 422
  • [8] Silica sulfuric acid as an efficient catalyst for the preparation of 2 H -indazolo[2,1- b]phthalazine-triones[J] . Hamid Reza Shaterian,Majid Ghashang,Mostafa Feyzi.Applied Catalysis A, General . 2008 (2)
  • [9] A facile and efficient pinacol–pinacolone rearrangement of vicinal diols using ZnCl 2 supported on silica as a recyclable catalyst[J] . Dharita J. Upadhyaya,Shriniwas D. Samant.Applied Catalysis A, General . 2008 (1)
  • [10] Trityl chloride as a novel and efficient organic catalyst for room temperature preparation of bis(indolyl)methanes under solvent-free conditions in neutral media
    Khalafi-Nezhad, A.
    Parhami, A.
    Zare, A.
    Zare, A. R. Moosavi
    Hasaninejad, A.
    Panahi, F.
    [J]. SYNTHESIS-STUTTGART, 2008, (04): : 617 - 621