Syntheses, Crystal Structures, Thermal and Fluorescent Properties of Two New Bearing Bi(Ⅲ) Supramolecular Compounds

被引：0

作者：

卢伟红 ^{[1
,2
]}

许婷 ^{[1
,2
]}

阳帆 ^{[1
,2
]}

孙俊彬 ^{[1
,2
]}

陈满生 ^{[1
,2
]}

颜群轩 ^{[3
]}

机构：

[1] Key Laboratory of Functional Metal-organic Compounds of Hunan Province & Key Laboratory of Functional Organometallic Materials of Hunan Province College

[2] Department of Chemistry and Materials Science, Hengyang Normal University

[3] Hunan Jinkai Recycling Technology Co.LTD

来源：

Chinese Journal of Structural Chemistry | 2021年 / 40卷 / 05期

关键词：

Bi(Ⅲ) supramolecular compounds; crystal structure; fluorescence; thermal stability;

D O I：

10.14102/j.cnki.0254-5861.2011-2983

中图分类号：

O641.4 [络合物化学（配位化学）];

学科分类号：

070304 ; 081704 ;

摘要：

Two new bearing Bi(Ⅲ) supramolecular compounds [Bi(pydcH)3(Bi(pydcH)(pydcH2)(pydc)(Bi(pydcH)(pydcH2)(pydc)](1) and {[Bi(pydcH)3]·(H2O)5(Dmap)}2(2) have been successfully synthesized via hydrothermal reaction(pydcH2= 2,6-pyridine dicarboxylate, Dmap = 4-dimethylamiopyridine). They have been structurally determined by single-crystal X-ray analysis, and characterized by fluorescence analysis and thermogravimetric analysis(TG). Both compounds 1 and 2 are of the same triclinic system with different structures. The decomposition mechanisms of compounds 1 and 2 are discussed. Compared to 1, lots of small molecules were possibly removed from compound 2 below 250 ℃. In addition, the photoluminescence properties were also investigated.

引用

页码：603 / 609

页数：7

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