Synthesis and Crystal Structure of N′-(4-fluorobenzylidene)-2-(1H-1,2,4-triazole-1-yl)acetohydrazide

被引：0

作者：

LI Weihua ZHANG Shufang HOU Baorong and YU Zhigang Institute of Oceanology Chinese Academy of Sciences Qingdao P R China College of Chemistry and Chemical Engineering Ocean University of China Qingdao P R China ^{[1
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机构：

来源：

ChemicalResearchinChineseUniversities | 2006年 / 05期

关键词：

1H-1,2,4-Triazole; Acetohydrazide; Crystal structure; Biological activity;

D O I：

暂无

中图分类号：

O626.2 [含双或多异原子的五节杂环];

学科分类号：

070303 ; 081704 ;

摘要：

N′-（4-fluorobenzylidene）-2-（1H-1,2,4-triazole-1-yl） acetohydrazide was synthesized by the reaction of 4-fluorobenzaldehyde with 2-（1H-1,2,4-triazole-1-yl） acetohydrazide. The structure was confirmed via elemental analysis, MS, 1H NMR, IR, and X-ray diffraction. It crystallized in a monoclinic system with space group P2（1）, a=0.4905（1） nm, b=0.8160（2） nm, c=1.4105（3） nm, β=93.33（3）°, Z=2, V=0.5636（2） nm 3, D_ c=1.457 Mg/m 3, μ=0.112 mm -1, F（000）=256, and final R_ 1=0.0685. Several intermolecular hydrogen-bond interactions existed in the crystal structure, facilitating the stabilization of the compound.

引用

页码：571 / 573

页数：3