Synthesis of new hyodeoxycholic acid thiosemicarbazone derivatives under solvent-free conditions using microwave

被引:0
作者
Zhi Chuan Shi
机构
关键词
Thiosemicarbazone; Steroids; Hyodeoxycholic acid; Antimicrobial activity; Microwave;
D O I
暂无
中图分类号
O621.3 [有机合成化学];
学科分类号
070303 ; 081704 ;
摘要
An efficient and simple method for synthesis of new hyodeoxycholic acid thiosemicarbazone derivatives under solvent-free conditions using microwave has been developed.Its main advantages are short reaction times,good conversions and the environmentally friendly nature of the process.The preliminary results indicate that some of these compounds possess inhibitory effects against E.coli.
引用
收藏
页码:405 / 408
页数:4
相关论文
共 50 条
  • [1] Synthesis of new hyodeoxycholic acid thiosemicarbazone derivatives under solvent-free conditions using microwave
    Shi, Zhi Chuan
    Zhao, Zhi Gang
    Liu, Xing Li
    Chen, Yu
    CHINESE CHEMICAL LETTERS, 2011, 22 (04) : 405 - 408
  • [2] Rapid and Efficient Synthesis of New Deoxycholic Acid Thiosemicarbazone Derivatives under Solvent-Free Conditions using Microwaves
    Shi, Zhi-Chuan
    Zhao, Zhi-Gang
    Liu, Xing-Li
    Qiu, Li-Ying
    LETTERS IN ORGANIC CHEMISTRY, 2011, 8 (07) : 515 - 519
  • [3] Microwave Assisted Solvent-Free Synthesis of Novel Chenodeoxycholic Acid Thiosemicarbazone Derivatives and Studies on Antibacterial Activities
    Zhao, Zhi-Gang
    Yan, Ping
    Liu, Xing-Li
    Shi, Zhi-Chuan
    LETTERS IN ORGANIC CHEMISTRY, 2012, 9 (08) : 604 - 608
  • [4] Rapid and Efficient Synthesis of Ester-Type Molecular Tweezers Derived from Hyodeoxycholic Acid in Solvent-Free Conditions under Microwave Irradiation
    Wu, Xiuming
    Zhao, Zhigang
    Liu, Xingli
    Chen, Yu
    Zhao, Xiaoxiang
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2009, 29 (06) : 956 - 961
  • [5] Microwave synthesis of metal phthalocyanines under solvent-free conditions
    Ki Suck Jung
    Jong Ho Kwon
    Se Mo Shon
    Jin Phil Ko
    Jun Sik Shin
    Seong Soo Park
    Journal of Materials Science, 2004, 39 : 723 - 726
  • [6] Synthesis of ferrocenyl Schiff bases under solvent-free conditions using microwave irradiation
    Ozturk, Gulsen
    Petit, Alain
    Kouklovsky, Cyrille
    SYNTHETIC COMMUNICATIONS, 2008, 38 (16) : 2707 - 2713
  • [7] Microwave-assisted synthesis of cinnamic acid derivatives in the presence of PPE and under solvent-free condition
    Mobinikhaledi, A.
    Foroughifar, N.
    Jirandehi, H. Fathinejad
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2008, 38 (05) : 428 - 430
  • [8] Solvent and solvent-free multistep synthesis under microwave activation
    Bataille, X
    Przedpelska, E
    Ziminska, M
    ACTUALITE CHIMIQUE, 2005, : 40 - 47
  • [9] Erlenmeyer azlactone synthesis with aliphatic aldehydes under solvent-free microwave conditions
    Chandrasekhar, Sosale
    Karri, Phaneendrasai
    TETRAHEDRON LETTERS, 2007, 48 (05) : 785 - 786
  • [10] Solvent-free synthesis of novel phthalocyanines containing triazole derivatives under microwave irradiation
    Ozil, Musa
    Canpolat, Mutlu
    POLYHEDRON, 2013, 51 : 82 - 89