Hydrothermal synthesis method of 5-(4'-methylbiphenyl-2-yl)-1H-tetrazole

被引：0
作者：
Wen-Xiang Wang [1 ]
Hong-Ling Cai [1 ]
Ren-Gen Xiong [1 ]
机构：
[1] Ordered Matter Science Research Center, Southeast University
来源：
Chinese Chemical Letters | 2013年 / 09期
关键词：
Tetrazole; Hydrothermal synthesis; Propane-1,2-diol; Sartan;
D O I：
暂无
中图分类号：
O621.3 [有机合成化学];
学科分类号：
070303 ; 081704 ;
摘要：
A clean and safe synthesis method of 5-(4’-methylbiphenyl-2-yl)-1H-tetrazole was found:under hydrothermal conditions,1.2 equiv.of 4’-methylbiphenyl-2-carbonitrile react with 1 equiv.of sodium azide in a mixed solvent of propane-1,2-diol/H2O,with 1.5 equiv.of ammonium chloride and 0.2 equiv.of ammonium fluoride as catalyst.After simple post-processing,the yield can be improved to 95%,and the purity of the product is 99%without further recrystallization.
引用
收藏
页码：783 / 785
页数：3
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