Synthesis, Crystal Structure, and Biological Activities of 2-Oxo-2-aryl-1-(1,2,4-triazol-1-yl)ethyl phenylcarbamodithioate

被引：0

作者：

XU Liangzhong ZHOU Kai HU Zhiqiang and BI Wenzhao College of Chemistry and Molecular Engineering Qingdao University of Science and Technology Qingdao P R China ^{[266042
]}

机构：

来源：

ChemicalResearchinChineseUniversities | 2006年 / 06期

关键词：

1,2,4-Triazole; Crystal structure; Biological activity;

D O I：

暂无

中图分类号：

O621.25 [];

学科分类号：

070303 ; 081704 ;

摘要：

The two title compounds, 2-oxo-2-p-tolyl-1-（1,2,4-triazol-1-yl）ethyl phenylcarbamodithioate（compound 3a） and 2-oxo-2-p-biphenyl-1-（1,2,4-triazol-1-yl）ethyl phenylcarbamodithioate（compound 3b）, were synthesized and {identified} by IR, EA and {}1H NMR spectra. The crystal structure of compound 3b was determined by X-ray diffraction analysis. The compound crystallized in a monoclinic system of space group P21/c with Mr=398.47（C_ 23 H_ 18 N4OS）, a=0.8769（2） nm, b=1.1924（2） nm, c=2.0440（6） nm, β=109.66（3）°, V=2.0126（8） nm3, Z=4, Dc=1.315 g/cm3, F（000）=832, μ=0.183 mm~ -1 , final R1=0.0819. The biological test result shows that the two title compounds exhibit certain fungicidal activities.

引用

页码：765 / 767

页数：3

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