Yttriumaluminumgarnet(Y3Al5O12)nanopowderssynthesizedbythechemicalmethod

被引：0

作者：

ZHANG Huashan SU Chunhui HAN Hui HOU Zhaoxia and WANG Guangzhao School of Materials Changchun University of Science and Technology Chuangchun China The First Research Laboratory China North Vehicle Research Institute Beijing China ^{[1
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机构：

来源：

Rare Metals | 2005年 / 02期

关键词：

inorganic materials; yttrium aluminum garnet nanopowders; citrate-gel method; low temperature self-propagating combustion reaction;

D O I：

暂无

中图分类号：

TB383 [特种结构材料];

学科分类号：

070205 ; 080501 ; 1406 ;

摘要：

The homogeneously dispersed, less agglomerated YAG nanopowders are synthesized by the citrate-gel method followed by low-temperature self-propagating combustion reaction, using Y2O3, Al(NO3)3?9H2O and citric acid as starting materials. This method effectively solves the problems caused by solid-state reaction at high temperature and the hard ag-glomerates brought by the chemical precipitation method. The powders are characterized by TG-DTA, XRD, FT-IR and TEM respectively. The experiments show that the forming temperature of YAG crystal phase is 850°C and the pseudo-YAG crystalline appears during the calcination and transforms to pure YAG at 1050°C. The powders with sizes less than 50 nm are observed by TEM micrography, which is consistent with the result calculated by Scherrer's formula. The powders consist of single grains.

引用

页码：166 / 169+184 +184

页数：5