Synthesis and Crystal Structure of Ethyl 4-(3,4-Methylenedioxylphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyridine-5-carboxylate under Microwave Irradiation

被引：0
作者：
TU Shu-Jiang GAO Yuan ZHOU Jian-Feng SHI Da-Qing WANG Xiang-Shan ZHUANG Qi-Ya(Department of Chemistry
机构：
来源：
结构化学 | 2002年 / 06期
关键词：
1; 4-dihydropyridine; synthesis; microwave irradiation; crystal structure;
D O I：
10.14102/j.cnki.0254-5861.2002.06.006
中图分类号：
O623 [脂肪族化合物（无环化合物）];
学科分类号：
070303 ; 081704 ;
摘要：
The crystal structure of the title compound (C16H17NO5) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group C2/c with a = 18.520(2), b = 7.8910(1), c = 21.728(3) A, β = 104.77(1)°, V= 3070.4(7) A3, Mr= 303.31, Z = 8, Dc= 1.312 g/cm3, λ = 0.71073 A,μ(MoKα) = 0.098 mm-1 and F(000) = 1280. The structure was refined to R = 0.0486 and wR = 0.1287. There exist intermolecular hydrogen bonds in the crystal.
引用
收藏
页码：609 / 612
页数：4
相关论文
共 50 条
  • [31] Crystal structure and Hirshfeld surface analysis of ethyl 2′-amino-5-bromo-3′-cyano-6′-methyl-2-oxo-spiro[indoline-3,4′-pyran]-5′-carboxylate
    Naghiyev, Farid N.
    Khrustalev, Victor N.
    Venskovsky, Nikolai U.
    Akkurt, Mehmet
    Khalilov, Ali N.
    Bhattarai, Ajaya
    Mamedov, Ibrahim G.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 942 - +
  • [32] Synthesis and crystal structure of 4-(3-methoxyl-4-hydroxyl)-phenyl-methene-3-methyl-1-phenyl-5-pyrazolone under microwave irradiation
    Gao, Y
    Tu, SJ
    Feng, YJ
    Shi, DQ
    Wang, XS
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 22 (04) : 469 - 472
  • [33] Synthesis and Crystal Structure of 1-Phenyl-3-methyl-4-(4-bromophenyl)-6-(2-chlorophenyl)- pyrazolo[3,4-b] Pyridine under Microwave Irradiation
    ZOU Xianga
    Chinese Journal of Structural Chemistry, 2005, (01) : 109 - 113
  • [34] Methyl 6-Methyl-1-(4-methylphenyl)-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate
    Chen, Qing
    Liu, Qingjian
    Wang, Haiping
    MOLBANK, 2012, (02)
  • [35] Synthesis and crystal structure of 1-phenyl-3-methyl-4-(4-bromophenyl)-6-(2-chlorophenyl)-pyrazolo[3,4-b] pyridine under microwave irradiation
    Zou, X
    Tu, SJ
    Zhu, SL
    Ji, SJ
    Zhang, Y
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2005, 24 (01) : 109 - 113
  • [36] Crystal structure of ethyl 2-(4-chlorophenyl)-3-cyclopentyl-4-oxo-1-propylimidazolidine-5-carboxylate
    Tabarki, Mohamed Ali
    Ben Smida, Youssef
    Guesmi, Abderrahmen
    Besbes, Rafaa
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O682 - +
  • [37] Synthesis and crystal structure of 2,7,7-trimethyl-3-ethoxycarbonyl-4-(3-nitrophenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline under microwave irradiation
    Tu, SJ
    Yu, CX
    Liu, XH
    Yao, CS
    Liu, F
    Gao, Y
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2002, 21 (01) : 99 - 102
  • [38] Synthesis and Crystal Structures of Methyl 3-(Benzoylamino)-6-methyl-2-oxo-2H-pyran-5-carboxylate and N-[5-(3,4-Dimethoxyphenyl)-6-methyl-2-oxo-2H-pyran-3-yl]benzamide
    Kranjc, Kristof
    Juranovic, Amadej
    Kocevar, Marijan
    Perdih, Franc
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2012, 42 (05) : 443 - 449
  • [39] Synthesis and Crystal Structures of Methyl 3-(Benzoylamino)-6-methyl-2-oxo-2H-pyran-5-carboxylate and N-[5-(3,4-Dimethoxyphenyl)-6-methyl-2-oxo-2H-pyran-3-yl]benzamide
    Krištof Kranjc
    Amadej Juranovič
    Marijan Kočevar
    Franc Perdih
    Journal of Chemical Crystallography, 2012, 42 : 443 - 449
  • [40] Ethyl 4-(2-fluorophenyl)-6-methyl-2-thioxo-1-(p-tolyl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
    Goncalves, Itamar Luis
    Kagami, Luciano Porto
    das Neves, Gustavo Machado
    Rockenbach, Liliana
    Davi, Leonardo
    Soares, Alceu Felipe
    Garcia, Solange Cristina
    Eifler-Lima, Vera Lucia
    MOLBANK, 2018, (04)
12345