Synthesis and Crystal Structure of Ethyl 4-(3,4-Methylenedioxylphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyridine-5-carboxylate under Microwave Irradiation

被引：0

作者：

TU ShuJiang GAO Yuan ZHOU JianFeng SHI DaQing WANG XiangShan ZHUANG QiYaDepartment of Chemistry Xuzhou Normal University Xuzhou Jiangsu ChinaDepartment of Chemistry Shenzhen University Shenzhen China Department of Chemistry Huaiyin Teacher College Huaiyin Jiangsu China ^{[221009
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机构：

来源：

结构化学 | 2002年 / 06期

关键词：

1; 4-dihydropyridine; synthesis; microwave irradiation; crystal structure;

D O I：

10.14102/j.cnki.0254-5861.2002.06.006

中图分类号：

O623 [脂肪族化合物（无环化合物）];

学科分类号：

070303 ; 081704 ;

摘要：

<正>The crystal structure of the title compound (C16H17NO5) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group C2/c with a = 18.520(2), b = 7.8910(1), c = 21.728(3) A, β = 104.77(1)°, V= 3070.4(7) A3, Mr= 303.31, Z = 8, Dc= 1.312 g/cm3, λ = 0.71073 A,μ(MoKα) = 0.098 mm-1 and F(000) = 1280. The structure was refined to R = 0.0486 and wR = 0.1287. There exist intermolecular hydrogen bonds in the crystal.

引用

页码：609 / 612

页数：4