Synthesis and Crystal Structure of Ethyl 4-(3,4-Methylenedioxylphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyridine-5-carboxylate under Microwave Irradiation

被引：0

作者：

TU Shu-Jiang GAO Yuan ZHOU Jian-Feng SHI Da-Qing WANG Xiang-Shan ZHUANG Qi-Ya(Department of Chemistry

机构：

来源：

结构化学 | 2002年 / 06期

关键词：

1; 4-dihydropyridine; synthesis; microwave irradiation; crystal structure;

D O I：

10.14102/j.cnki.0254-5861.2002.06.006

中图分类号：

O623 [脂肪族化合物（无环化合物）];

学科分类号：

070303 ; 081704 ;

摘要：

The crystal structure of the title compound (C16H17NO5) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group C2/c with a = 18.520(2), b = 7.8910(1), c = 21.728(3) A, β = 104.77(1)°, V= 3070.4(7) A3, Mr= 303.31, Z = 8, Dc= 1.312 g/cm3, λ = 0.71073 A,μ(MoKα) = 0.098 mm-1 and F(000) = 1280. The structure was refined to R = 0.0486 and wR = 0.1287. There exist intermolecular hydrogen bonds in the crystal.

引用

页码：609 / 612

页数：4

共 50 条

[1] Synthesis and crystal structure of ethyl 4-(3,4-methylenedioxylphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyridine-5-carboxylate under microwave irradiation
Tu, SJ
Gao, Y
Zhou, JF
Shi, DQ
Wang, XS
Zhuang, QY
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2002, 21 (06) : 609 - 612
[2] Synthesis under microwave irradiation and crystal structure of 4-(3,4-methylenedioxylphenyl)-6-methyl-5-ethoxycaronyl-3,4-dihydropyrimidin-2(H)-one
Tu, SJ
Fang, F
Jiang, H
Zhu, SL
Li, TJ
Zhang, XJ
Shi, DQ
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (05) : 494 - 497
[3] Synthesis under Microwave Irradiation and Crystal Structure of 4-(3,4-Methylenedioxylphenyl)-6-methyl- 5-ethoxycaronyl-3,4-dihydropyrimidin-2(H)-one
TU Shu-Jiang② FANG Fang JIANG Hong ZHU Song-Lei LI Tuan-Jie ZHANG Xiao-Jing SHI Da-Qing (Department of Chemistry
Key Laboratory of Biotechnology on Medical Plant of Jiangsu Province
结构化学, 2004, (05) : 494 - 497
[4] Crystal structure of methyl 4-(4-hydroxyphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate monohydrate
Bairagi, Keshab M.
Venugopala, Katharigatta N.
Mondal, Pradip Kumar
Odhav, Bharti
Nayak, Susanta K.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 1335 - +
[5] Crystal structures of the anhydrous and two solvated forms of methyl 4-(4-fluorophenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Cleetus, Annie
Rani, Gulshan
Rao, G. B. Dharma
Chopra, Deepak
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2020, 76 : 786 - +
[6] Crystal structure of ethyl 6-methyl-2-oxo-4-(3,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Novina, J. J.
Vasuki, G.
Suresh, M.
Padusha, M. Syed Ali
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O206 - +
[7] Crystal structure of ethyl 6-(chloromethyl)-4-(4-chlorophenyl)-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Bharanidharan, S.
Saleem, H.
Gunasekaran, B.
Padusha, M. Syed Ali
Suresh, M.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1185 - +
[8] Crystal structure of ethyl 4-(2-methoxy-phenyl)-6-methyl-2-sulfanylidene-1,2,3,4- tetrahydropyrimidine-5-carboxylate
Mohamed, Shaaban K.
Mague, Joel T.
Akkurt, Mehmet
Khodairy, Ahmed
Ahmed, Eman A.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O444 - U140
[9] Synthesis and crystal structure of 4-(2-chlorophenyl)-5-cyano-3-methyl-6-oxo-1-phenyl-4,5,6,7-tetrahydropyrazolo[3,4-b] pyridine under microwave irradiation
Zhu, SL
Tu, SJ
Li, TJ
Zou, X
Zhang, XJ
Ji, SJ
Zhang, Y
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (11) : 1222 - 1225
[10] Crystal structure of ethyl 4-(2-fluoro-phenyl)-6-methyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Krishnamurthy, M. S.
Begum, Noor Shahina
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O699 - U139

← 1 2 3 4 5 →