Synthesis, Crystal Structure and Luminescent Property of a Ag(Ⅰ) Coordination Polymer with a 3D Sandwich-like Framework

被引：11
|
作者：
LU Jiu-Fu [1 ]
SHI Juan [1 ]
ZHENG Nan [1 ]
GUO Xiao-Hua [1 ]
GE Hong-Guang [1 ]
机构：
[1] Chemical Engineering College,Shaanxi University of Technology
来源：
结构化学 | 2016年 / 35卷 / 02期
基金：
中国国家自然科学基金;
关键词：
Ag(Ι) coordination polymer; crystal structure; luminescent property;
D O I：
10.14102/j.cnki.0254-5861.2011-0814
中图分类号：
O634 [元素有机聚合物];
学科分类号：
摘要：
A new coordination polymer,{[Ag(bpp)(HO)]·bpdc·3HO},derived from the ligand biphenyl-4,4’-dicarboxylic acid(Hbpdc),has been obtained through a hydrothermal technique(bpp = l,3-bis(4-pyridyl)propane).Its single-crystal structure has been characterized by single-crystal X-ray diffraction,powder XRD,FT-IR,TGA and elemental analysis techniques.The single-crystal X-ray diffraction reveals that complex 1 consists of 1D infinite[Ag(bpp)(HO)]cationic chains,2D anionic layer constructed by bpdc anions and free water which provide charge compensation in the crystal structure.The 1D infinite[Ag(bpp)(HO)]cationic chains and 2D anionic layer are further stacked in-ABAB- fashion through intermolecular H-bonding to form a 3D sandwich-like framework.In addition,the luminescent property of complex 1 in the solid state at room temperature was investigated.
引用
收藏
页码：319 / 325
页数：7
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