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On-line Sweeping Sample Concentration in Micellar Electrokinetic Chromatography with Enhanced Sensitivity for the Deter-mination of Carbamazepine in Human Serum
被引：0
作者：
Dan Dan HAN1
机构：
关键词：
On-line concentration;
carbamazepine;
MEKC;
sweeping;
human serum;
D O I：
暂无
中图分类号：
R96 [药理学];
学科分类号：
100602 ;
100706 ;
摘要：
A sensitive and simple micellar electrokinetic chromatography (MEKC) method was developed for the determination of antiepileptic drug,carbamazepine (CBZ),using sweeping on-line concentration method with photodiode array detection. Under the optimal conditions,the calibration curve was linear over a range of 0.5-40 μg·mL-1 for CBZ with a correlation coefficient of 0.998. The detection limit (S/N = 3:1) of CBZ was 0.10 μg·mL-1. The sweeping-MEKC method has been successfully applied to the analysis of CBZ in human serum.
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页码：953 / 956
页数：4
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