Synthesis and Crystal Structure of 3,5-Dichloro-N-(2-methoxyphenyl)benzamide

被引：1

作者：

Aamer Saeed ^{[1
]}

Ulrich Flrke ^{[2
]}

机构：

[1] Department of Chemistry, Quaid-I-Azam University

[2] Department Chemie, Fakultt fur Naturwissenschaften, Universitt Paderborn

来源：

结构化学 | 2013年 / 32卷 / 02期

关键词：

chlorinated benzamide; synthesis; crystal structure;

D O I：

10.14102/j.cnki.0254-5861.2013.02.016

中图分类号：

O625.6 [芳香族含氮化合物];

学科分类号：

070303 ; 081704 ;

摘要：

The title compound was synthesized by the direct reaction of 3,5-dichlorobenzoic acid with 2-methoxyaniline in the presence of DCC and HOBT. The structure was supported by the spectroscopic data and unambiguously confirmed by the single-crystal X-ray diffraction studies. It crystallizes from a methanol solution in the monoclinic space group P2;/c with unit cell dimensions of a = 4.9369（16）, b = 13.351（5）, c = 20.168（7）, β = 96.755（8）°, V = 1320.1（8）;and Z = 4.

引用

页码：211 / 214

页数：4

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