Chemical component analysis of volatile oil in drug pair Herba Ephedrae-Ramulus Cinnamomi by GC-MS and CRM

被引：0

作者：

陈勇 ^{[1
]}

李晓如 ^{[2
]}

赵君 ^{[2
]}

周涛 ^{[2
]}

邹桥 ^{[2
]}

机构：

[1] The Second Xiangya Hospital, Central South University 2. School of Chemistry and Chemical Engineering, Central South University

来源：

Journal of Central South University of Technology | 2007年 / 04期

关键词：

drug pair (DP); Herba Ephedrae-Ramulus Cinnamomi; volatile oil; gas chromatography/mass spectrometry (GC-MS); chemometric resolution method (CRM);

D O I：

暂无

中图分类号：

O657.63 [质谱分析];

学科分类号：

070302 ; 081704 ;

摘要：

Active volatile components in drug pair(DP)Herba Ephedrae-Ramulus Cinnamomi(HE-RC),single drug HE and RC were analyzed by gas chromatography/mass spectrometry(GC/MS),chemometric resolution method(CRM)and overall volume integration.By means of CRM,the two-dimensional data obtained from GC-MS instruments were resolved into a pure chromatogram and a mass spectrum of each chemical compound.In total,97,62,and 78 volatile chemical components in volatile oil of HE,RC,and DP HE-RC,were respectively determined qualitatively and quantitatively,accounting for 90.08%,91.62%,and 89.76% total contents of volatile oil of HE,RC,and DP HE-RC respectively.It is further demonstrated that the numbers of volatile components of DP HE-RC are almost the sum of those of two single drugs,but some relative contents of them are changed.Some new components,such as 1,6-dimethylhepta-1,3,5-triene,tetracyclo[4.2.1.1(2,5).0(9,10)]deca-3,7-diene,globulol and(E,E)-6,10,14-trimethyl-5,9,13-pentadecatrien-2-one are found in DP HE-RC because of chemical reactions and physical changes during decoction.

引用

页码：509 / 513

页数：5

共 4 条

[1]

Analysis of volatile chemical components of Radix Paeoniae Rubra by gas chromatography-mass spectrometry and chemometric resolution[J] . Xiao-ru Li,Zheng-gang Lan,Yi-zeng Liang.Journal of Central South University of Technology . 2007 (1)

[2] Determination of constituents of essential oil from Angelica sinensis by gas chromatography -: mass spectrometry [J].

Wu, MJ ;

Sun, XJ ;

Dai, YH ;

Guo, FQ ;

Huang, LF ;

Liang, YZ .

JOURNAL OF CENTRAL SOUTH UNIVERSITY OF TECHNOLOGY, 2005, 12 (04) :430-436

[3]

Determination of volatile components in peptic powder by gas chromatography–mass spectrometry and chemometric resolution[J] . Fan Gong,Yi-Zeng Liang,Hui Cui,Foo-Tim Chau,Benny Tsz-Pun Chan.Journal of Chromatography A . 2001 (2)

[4]

Gas chromatography–mass spectrometry and chemometric resolution applied to the determination of essential oils in Cortex Cinnamomi[J] . Fan Gong,Yi-Zeng Liang,Qing-Song Xu,Foo-Tim Chau.Journal of Chromatography A . 2001 (1)

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