Two highly porous single-crystalline zirconium-based metal-organic frameworks

被引：0

作者：

Wen-Yang Gao ^{[1
]}

Timmy Thiounn ^{[1
]}

Lukasz Wojtas ^{[1
]}

Yu-Sheng Chen ^{[2
]}

Shengqian Ma ^{[1
]}

机构：

[1] Department of Chemistry, University of South Florida

[2] ChemMatCARS, Center for Advanced Radiation Sources, University of Chicago

来源：

Science China(Chemistry) | 2016年 / 08期

基金：

美国国家科学基金会;

关键词：

metal-organic frameworks; zirconium cluster; single-crystalline;

D O I：

暂无

中图分类号：

O627 [元素有机化合物];

学科分类号：

070303 ; 081704 ;

摘要：

Herein we report two highly porous Zr-based metal-organic frameworks（MOFs, 1 and 2） constructed by the truncated octahedral secondary building unit（SBU） of Zr;O;（OH）;（CO;）;and the organic linear ligand of 4,4.-stilbenedicarboxylic acid（H;sbdc） or4,4′-azobenezenedicarboxylic acid（H;abdc）. Both Zr-based MOFs are obtained as single crystals of suitable size for single-crystal X-ray diffraction analysis. Furthermore, these two Zr-based MOFs have been fully characterized by powder X-ray diffraction（PXRD） studies, thermogravimetric analysis（TGA）, infrared spectroscopy（IR） and gas adsorption analysis. In particular, their CO;gas adsorption behaviors have been investigated and discussed.

引用

页码：980 / 983

页数：4

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