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Structural and Piezoelectric Properties of Sr0.6Ba0.4Nb2O6 Micro-rods Synthesized by Molten-Salt Method
被引:0
作者:
Zhang Guangbin
[1
]
Hu Chengchao
[2
]
Shi Yangguang
[1
]
Shi Daning
[1
]
机构:
[1] Department of Applied Physics,Nanjing University of Aeronautics and Astronautics
[2] College of Materials Science and Engineering,Liaocheng University
基金:
中国国家自然科学基金;
关键词:
Sr0.6Ba0.4Nb2O6;
micro-rods;
molten salt method;
X-ray diffraction patterns;
transmission electron microscope(TEM)imaging;
piezoresponse force microscope(PFM)detection;
D O I:
10.16356/j.1005-1120.2018.03.432
中图分类号:
TB34 [功能材料];
学科分类号:
080501 ;
摘要:
Sr0.6 Ba0.4 Nb2 O6 micro-rods are prepared by the molten-salt method with K2 SO4,KCl-K2 SO4,and KCl as fluxes.It reveals that the Sr0.6 Ba0.4 Nb2 O6 synthesized with KCl as a flux exhibits a single phase with tetragonal tungsten bronze structure.The measurement of X-ray diffraction indicates that the Sr0.6 Ba0.4 Nb2 O6 micro-rods synthesized at 1 300℃are anisotropic.The morphology of the powers is examined by transmission electron microscope.It reveals that the length-diameter ratio of Sr0.6 Ba0.4 Nb2 O6 micro-rods increases with increasing annealing temperature from 900℃to 1 300℃.At 1 300℃,the rod possesses a large length-diameter ratio of 8∶1.Moreover,the analysis of the piezoelectric properties of single micro-rods using apiezo-response force microscope indicates that the domains of the material are arranged along its radial direction.
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页码:432 / 436
页数:5
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