Crystal Structure of Phenol,2-[4(S)-4-Dihydro-4-benzyl-2-ozazolinyl]

被引：0

作者：

罗梅 ^{[1
]}

周仕明 ^{[2
]}

张家海 ^{[2
]}

庞文民 ^{[3
]}

尹浩 ^{[2
]}

胡克良 ^{[2
]}

机构：

[1] Hefei University of Technology,Department of Chemical Engineering

[2] University of Science and Technology,Department of Chemistry (Hefei)

[3] University of Science and Technology,Department of Chemistry (Hefei)

来源：

结构化学 | 2010年 / 29卷 / 06期

关键词：

oxazoline; phenol; 2-[4(S)-4; 5-dihydro-4-phenyl-2-ozazolinyl; (C15H13NO2); crystal structure;

D O I：

10.14102/j.cnki.0254-5861.2010.06.019

中图分类号：

O621.2 [有机化合物性质];

学科分类号：

070303 ; 081704 ;

摘要：

The compound phenol,2-[4(S)-4,5-dihydro-4-phenyl-2-ozazolinyl(1,C15H13NO2) was synthesized with a simple,one step method free of water and air.It was obtained in a moderate yield from the reaction of 2-hydroxybenzonitrile with optically active amino alcohol in chloroben-zene under dry,anaerobic conditions.It belongs to the orthorhombic system,space group P212121 with a = 5.786(5),b = 10.730(5),c = 19.722(5),C15H13NO2,Mr = 239.26,V = 1224.4(12)3,Z = 4 and Dc = 1.298 mg/m3.The final R = 0.0324 for 1627 observed reflections with Ⅰ > 2σ(Ⅰ) and Rw = 0.0826 for all data.The structure of compound 1 was determined by X-ray diffraction,NMR and HRMS.

引用

页码：947 / 949

页数：3

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