Inferential Online Measurement of 3D Fractal Dimension of Spray Fluidized Bed Agglomerates

被引:0
作者
Men, Jialin [1 ,2 ]
Ajalova, Aisel [2 ]
Tsotsas, Evangelos [2 ]
Bueck, Andreas [2 ]
机构
[1] Friedrich Alexander Univ Erlangen Nurnberg, Interfaces & Particle Technol, Cauerstr 4, D-91058 Erlangen, Germany
[2] Otto von Guericke Univ, Thermal Proc Engn, Univ pl 2, D-39106 Magdeburg, Germany
关键词
agglomeration; fluidized bed; image analysis; morphology; structure; MORPHOLOGY; TOMOGRAPHY;
D O I
10.3390/pr13072316
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
In this work, a model-based approach to inferentially obtaining information about the 3D fractal dimension of agglomerates produced in spray fluidized beds is presented. The method utilizes high-detail but scarce offline information from X-ray microcomputed tomography for establishing and training an inferential relationship with online information that is easy and fast to obtain. The online measurement information is the geometric roundness of the single agglomerate. To investigate the interpolation capability of the inferential approach, three different strategies are evaluated: correlation with individual process conditions; correlation with parameters adjusted to process parameters; and correlation with respect to a range of process conditions. It is shown that the approach incorporating process conditions provides sufficient accuracy over a wide range of conditions. The inferential evaluation of single agglomerate 3D fractal dimension is achieved in 5 ms on average. This enables the measurement of the distribution of 3D fractal dimension in an online setting for product quality monitoring and control. Several examples illustrate the capabilities of the approach, as well as current limitations.
引用
收藏
页数:14
相关论文
共 31 条
[11]   Use of X-ray tomography to study the porosity and morphology of granules [J].
Farber, L ;
Tardos, G ;
Michaels, JN .
POWDER TECHNOLOGY, 2003, 132 (01) :57-63
[12]   Experimental study and SEM-EDS analysis of agglomerates from gasification of biomass in fluidized beds [J].
Furuvik, Nora C. I. S. ;
Wang, Liang ;
Jaiswal, Rajan ;
Thapa, Rajan ;
Eikeland, Marianne S. ;
Moldestad, Britt M. E. .
ENERGY, 2022, 252
[13]   Fractal characteristic of recycled aggregate and its influence on physical property of recycled aggregate concrete [J].
Gao, Song ;
Li, Qiuyi ;
Luo, Jianlin .
REVIEWS ON ADVANCED MATERIALS SCIENCE, 2021, 60 (01) :663-677
[14]   Catalyst Supraparticles: Tuning the Structure of Spray-Dried Pt/SiO2 Supraparticles via Salt-Based Colloidal Manipulation to Control their Catalytic Performance [J].
Groppe, Philipp ;
Reichstein, Jakob ;
Carl, Simon ;
Cuadrado Collados, Carlos ;
Niebuur, Bart-Jan ;
Zhang, Kailun ;
Apeleo Zubiri, Benjamin ;
Libuda, Joerg ;
Kraus, Tobias ;
Retzer, Tanja ;
Thommes, Matthias ;
Spiecker, Erdmann ;
Wintzheimer, Susanne ;
Mandel, Karl .
SMALL, 2024, 20 (35)
[15]   AGGLOMERATION MODELS FOR PROCESS DESIGN AND CONTROL [J].
HOGG, R .
POWDER TECHNOLOGY, 1992, 69 (01) :69-76
[16]   Investigation of fluidized bed agglomerate growth process using simulations and SEM-EDX characterization of laboratory-generated agglomerates [J].
Khadilkar, Aditi B. ;
Rozelle, Peter L. ;
Pisupati, Sarma V. .
CHEMICAL ENGINEERING SCIENCE, 2018, 184 :172-185
[17]  
Koerfer R, 2008, INF TECHNOL CONTROL, V37, P285
[18]   Optical characterisation of polymeric nanocomposites using tomographic, spectroscopic and Fraunhofer wavefront assessment [J].
Koukoulas, Triantafillos ;
Broughton, William R. ;
Williams, John ;
Rahatekar, Sameer .
OPTICAL SYSTEMS DESIGN 2012, 2012, 8550
[19]   Characterisation of soot in oil from a gasoline direct injection engine using Transmission Electron Microscopy [J].
La Rocca, A. ;
Bonatesta, F. ;
Fay, M. W. ;
Campanella, F. .
TRIBOLOGY INTERNATIONAL, 2015, 86 :77-84
[20]   Characterization of structure and mixing in nanoparticle hetero-aggregates using convolutional neural networks: 3D-reconstruction versus 2D-projection [J].
Mahr, Christoph ;
Stahl, Jakob ;
Gerken, Beeke ;
Krause, Florian F. ;
Schowalter, Marco ;
Grieb, Tim ;
Maedler, Lutz ;
Rosenauer, Andreas .
ULTRAMICROSCOPY, 2024, 265