Three kinds of SMAs with different composition Fe-30Mn-6Si, Fe-30Mn-6Si-1Ni, and Fe-30Mn-6Si-1Ni-1Ti were prepared with melt spinning. The microstructure of these alloys were analysed with X-ray diffraction (XRD), optical microscope (OM) and scanning-electron microscope (SEM), the shape recovery strain of the alloys were measured by tensile test. Dendrite spikes appears in Fe-30Mn-6Si, the dendrite arm spacing was about 0.2 μm. Equiaxial austenite grains distributed uniformly in Fe-30Mn-6Si-1Ni and Fe-30Mn-6Si-1Ni-1Ti, the grain size in Fe-30Mn-6Si-1Ni-1Ti was bigger. When the pre-strain was 1% and 1.5%, the shape recovery strain of Fe-30Mn-6Si-1Ni was higher than Fe-30Mn-6Si-1Ni-1Ti. When the pre-strain was 2%, the shape recovery strain of Fe-30Mn-6Si-1Ni-1Ti is higher than Fe-30Mn-6Si-1Ni. The Fe-30Mn-6Si-1Ni-1Ti shows the highest shape recovery strain 2% when then pre-strain was 3%. ©, 2015, Journal of Functional Materials. All right reserved.