共 47 条
Surface Modification of Poly(ethylene-alt-tetrafluoroethylene) by Atmospheric Pressure Dielectric Barrier Discharge Plasma
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Yan, Xiaoshan
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Ji, Zuohui
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Res Inst Aerosp Special Mat & Proc Technol, Beijing 100074, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Li, Xiaopeng
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Zhao, Yue
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Li, Zhen
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Chen, Zhai
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China

Li, Heguo
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Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China
机构:
[1] Inst Chem Def, State Key Lab NBC Protect Civilian, Beijing 100191, Peoples R China
[2] Res Inst Aerosp Special Mat & Proc Technol, Beijing 100074, Peoples R China
来源:
关键词:
ETFE membrane;
DBD plasma;
surface modification;
hydrophilicity;
peel strength;
FILM SURFACES;
MEMBRANE;
ACID;
POLYMERIZATION;
POLYPROPYLENE;
OPTIMIZATION;
IMPROVEMENT;
NANOSCALE;
CELLS;
D O I:
10.3390/polym17111519
中图分类号:
O63 [高分子化学(高聚物)];
学科分类号:
070305 ;
080501 ;
081704 ;
摘要:
The fluororesin membrane emerges as an ideal chemical-protective clothing material due to its excellent permeation resistance. However, using a fluororesin membrane with a low surface energy for compounding fabrics is very challenging. Herein, we demonstrate a strategy to modify the surface of a poly(ethylene-alt-tetrafluoroethylene) (ETFE) membrane by the atmospheric pressure dielectric barrier discharge (DBD) of plasma under different working voltages, processing times, and concentrations of acrylic acid (AA) in a helium (He) atmosphere. The increase in the hydrophilicity of the ETFE membrane is confirmed by the wettability test, which shows a significant decrease in the water contact angle, from 96 degrees to 50 degrees, after plasma modification. The interfacial T-peel strength of an ETFE membrane composited with polyester fabric increased from 0.53 N/cm to 13.64 N/cm after plasma modification. Significantly, the T-peel strength of the composite using a modified ETFE membrane with ultrasonic washing could still reach 11.75 N/cm. Various characterization methods clearly disclosed the physical and chemical changes on the ETFE membrane surface, such as introducing the polar -COOH group at a nano-level, improving the roughness, decreasing the ratios of the F/C element, and increasing the ratios of the O/C element, suggesting using nano-level grafted polyacrylic acid (g-PAA) on the surface of the membrane by DBD.
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页数:16
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