Carbon Thermal Reduction of Nickel Laterite Leaching Slag for Efficient Enrichment and Retrieval Efficiency of Iron

被引:0
作者
Li, Tingshuai [1 ]
Wu, Yusheng [1 ]
Wang, Yuzheng [1 ]
Liu, Feng [1 ]
Li, Laishi [1 ]
机构
[1] Shenyang Univ Technol, Sch Mat Sci & Engn, Shenyang 110870, Liaoning, Peoples R China
基金
中国国家自然科学基金;
关键词
STATE METALIZED REDUCTION; EFFECTIVE SEPARATION; MAGNETIC SEPARATION; ORE; FERRONICKEL; RECOVERY; CHROMIUM; RESIDUE; AGGREGATION; KINETICS;
D O I
10.1007/s11837-025-07483-z
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
As a representative solid waste in the domain of the nickel laterite ore industry, the resource utilization of nickel laterite leaching slag is always a difficult problem for the metallurgical industry. In this paper, the method of non-molten roasting reduction magnetic separation with anthracite as the reducing agent was investigated to enrich and recover iron from nickel laterite ore leaching slag. The reduction mechanism of the process was analyzed by thermodynamic calculations and equilibrium simulations of the physical phase. The effects of roasting temperature, holding time, and anthracite dosage on the conversion rate of iron-bearing minerals were studied. The response surface has been used to analyze the interaction of influencing factors. The optimum reduction conditions were: roasting temperature of 1320 degrees C, duration of 60 min, and reductant dosage of 25 wt.%. The iron purity and retrieval efficiency in the concentrate were 76.08% and 95.19%, respectively. The physical phase composition, microstructure, and magnetization intensity of the reduction products were studied by XRD, SEM-EDS, and VSM. The reduction mechanism of reactants and the aggregation process of products were studied.
引用
收藏
页码:5972 / 5983
页数:12
相关论文
共 32 条
[1]   Efficient recovery of iron and chromium from laterite residue by non-molten metallization reduction [J].
Cao, Zhihe ;
Ma, Baozhong ;
Zhou, Jiashun ;
Shi, Longfei ;
Chen, Yongqiang ;
Wang, Chengyan .
POWDER TECHNOLOGY, 2022, 407
[2]   Facile and inexpensive preparation method of iron phosphate from laterite residue [J].
Cao, Zhihe ;
Ma, Baozhong ;
Jing, Qiankun ;
Xing, Peng ;
Liu, Bao ;
Wang, Chengyan .
CERAMICS INTERNATIONAL, 2020, 46 (08) :11304-11310
[3]   Preparation of LiFePO4/C cathode material by extracting Fe2O3 from laterite nickel ore by ammonium jarosite method [J].
Chang, Longjiao ;
Wei, Anlu ;
Luo, Shaohua ;
Bi, Xiaolong ;
Yang, Wei ;
Yang, Ruifen ;
Liu, Jianan .
JOURNAL OF ALLOYS AND COMPOUNDS, 2023, 936
[4]   Pre-concentration of nickel in laterite ores using physical separation methods [J].
Farrokhpay, Saeed ;
Filippov, Lev ;
Fornasiero, Daniel .
MINERALS ENGINEERING, 2019, 141
[5]   The Aggregation and Growth of Ferronickel Particles During the Reduction of Laterite Nickel Ore [J].
Feng, Zhi ;
Li, Bo ;
Wei, Yonggang ;
Zhou, Shiwei .
JOURNAL OF SUSTAINABLE METALLURGY, 2023, 9 (03) :1099-1113
[6]   A study on separation of Mn and Fe from high-alumina ferruginous manganese ores by the carbothermal roasting reduction process [J].
Gao, Lihua ;
Liu, Zhenggen ;
Pan, Yuzhu ;
Feng, Cong ;
Ge, Yang ;
Chu, Mansheng .
ADVANCED POWDER TECHNOLOGY, 2020, 31 (01) :51-60
[7]   CO2 mineral sequestration and nickel recovery from laterite ore by using waste copperas [J].
Gao, Yuxiang ;
Jin, Xi ;
Teng, Liumei ;
Rohani, Sohrab ;
He, Minyu ;
Li, Jiangling ;
Ren, Shan ;
Liu, Qingcai ;
Huang, Junbin ;
Duan, Huamei ;
Xin, Yuntao ;
Liu, Weizao .
FUEL, 2023, 331
[8]   Mechanism of Calcium Sulphate on the Aggregation and Growth of Ferronickel Particles in the Self-Reduction of Saprolitic Nickel Laterite Ore [J].
Hang, Guihua ;
Xue, Zhengliang ;
Wang, Jinghui ;
Wu, Yingjiang .
METALS, 2020, 10 (04)
[9]   Extraction of ferronickel concentrate from laterite nickel ore by reduction roasting-magnetic separation using spent cathode carbon [J].
Hui, Shunyao ;
Li, Bo ;
Zhou, Shiwei ;
Wei, Yonggang .
MINERALS ENGINEERING, 2023, 201
[10]   Technospheric mining of scandium from hydrometallurgical tailings of nickel laterite processing: Selection of lixiviant and optimisation of leaching variables [J].
Ichlas, Zela T. ;
Jones, Sarah A. ;
Ibana, Don C. ;
Lee, Go-Gi ;
Alorro, Richard D. .
MINERALS ENGINEERING, 2022, 179