Properties and interfacial failure mode of surface modified polyimide fiber/epoxy composites

被引:0
作者
Qiu, Yang [1 ]
Li, Yafeng [1 ]
Tian, Guofeng [2 ]
Zhang, Mengying [3 ]
机构
[1] Composite Technology Center, AVIC Manufacturing Technology Institute, Beijing
[2] Beijing University of Chemical Technology, Key Laboratory of Carbon Fiber and Functional Polymers, Ministry of Education, Beijing
[3] Jiangsu Shino New Materials Technology Co. ,Ltd., Jiangsu, Changzhou
关键词
composites; epoxy; interface; plasma modification; polyimide fiber;
D O I
10.11868/j.issn.1001-4381.2023.000193
中图分类号
学科分类号
摘要
To solove the problem of the low surface energy of polyimide(PI) fiber and poor interfacial performance between PI fiber and epoxy, atmospheric air plasma was selected to modify the surface of PI fiber. The influence of treatment duration on the surface structure of PI fiber and the interfacial properties of PI/epoxy composites was investigated. Effects of atmospheric air plasma on the surface micromorphology of PI fiber and failure plane of PI/EP composites were observed by the SEM. Dynamic contact angle and lateral tow tensile strength tests were chosen to characterize the infiltration effect and interfacial performance between PI fiber and epoxy after plasma treatment. The flexural strength and interlaminar shear strength tests were selected as inspection items for composites performance. The results implicate that atmospheric air plasma treatment can increase the infiltration and interfacial connection between PI fiber and epoxy, the lateral tow tensile strength of PI fiber modified by plasma treatment for 6 min is 16.05 MPa, with increment of nearly 21%. The increases in flexural strength and interlaminar shear strength of PI/EP composites are 36.41% and 38.85% respectively. Atmospheric air plasma modification can remake the surface morphology of PI fiber,and improve the joining effect of PI fiber and epoxy. Furthermore,the failure model of PI/EP composites is transformed from interfacial failure to fiber surface failure. © 2024 Science Press. All rights reserved.
引用
收藏
页码:196 / 203
页数:7
相关论文
共 22 条
[1]  
MA P C, DAI C T, WANG H Zet al., A review on high temperature resistant polyimide films: heterocyclic structures and nanocomposites, Composites Communications, 16, pp. 84-93, (2019)
[2]  
B喏WANG R., Structures and properties of polyimide fibers and its applications [J], Hi-Tech Fiber & Application, 41, pp. 23-26, (2016)
[3]  
ZUO Q P喏LIN H喏CHEN Y Y., Progress in the development and application of polyimide fiber [J], China Textile Leader, pp. 60-63, (2018)
[4]  
ZHANG M, Research and applica⁃ tion of polyimide fibers with high strength and high modulus [J], In⁃ sulating Materials, 49, pp. 12-16, (2016)
[5]  
WANG B Y, ZHANG M Y, HAN E Let al., Mechanical behavior of polyimide filament tows under high strain rate tension, High Performance Polymers, 32, pp. 842-848, (2020)
[6]  
Y喏GAO H喏ZHANG ZHOU, Study on heat resistance and structural evolution of high-performance organic fibers [J], China Synthetic Fiber Industry, 42, pp. 6-14, (2019)
[7]  
Study on properties and mechanism of polyimide fiber reinforced epoxy resin structure wave-transmitting composites [J], China Adhesives2022, 31, pp. 1-5
[8]  
ZHANG Q, H喏CHEN D, J喏DING M X., Polyimide fibers [J], Poly⁃ mer Bulletin, pp. 66-73, (2001)
[9]  
pp. 19-27, (2017)
[10]  
LIAW D J, WANG K L, HUANG Y, Advanced polyimide materials:syntheses,physical properties and applications, Progress in Polymer Science, 37, pp. 907-974, (2012)