Characterization of the hydrothermal synthesis of uranium particles as a potential reference material for microanalysis methods

被引：0

作者：

Ruixuan Hu ^{[1
]}

Ningjie Zhong ^{[1
]}

Yan Shen ^{[1
]}

Shenghui Huang ^{[1
]}

Yan Zhang ^{[1
]}

Fangda Ren ^{[1
]}

Yonggang Zhao ^{[1
]}

机构：

[1] China Institute of Atomic Energy,Department of Radiochemistry

来源：

Journal of Radioanalytical and Nuclear Chemistry | 2025年 / 334卷 / 5期

关键词：

Particle analysis; Uranium-containing particles; Characterization; Reference materials; Nuclear safeguards; Hydrothermal synthesis;

D O I：

10.1007/s10967-025-10084-4

中图分类号：

学科分类号：

摘要：

In this study, micrometric uranium oxide particles produced by hydrothermal method were characterized. The applicability of the produced particles as reference materials for particle analysis, especially for mass spectrometry was evaluated in terms of morphology, size, isotope ratios, storage stability, and uranium yield. In addition, we compared the particles before and after heat treatment in air with the Nuclear Signatures Inter-laboratory Measurement Evaluation Programme-9 (NUSIMEP-9) particles. The results showed that the particles produced by hydrothermal method could meet the uniformity and stability of reference materials required for particle analysis.

引用

页码：3147 / 3155

页数：8

共 18 条

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