Natural acidic deep eutectic solvent-mediated microwave-assisted simultaneous hydrodistillation, hydrolysis, and extraction for obtaining essential oils, gallic acid and ellagic acid from Liquidambar formosana leaves and fruits

被引：2
作者：
Zhang, Ke [1 ]
Gao, Hongfei [1 ]
Yang, Yang [1 ]
Ping, Yifan [1 ]
Tian, Hao [2 ]
Gu, Huiyan [3 ]
Yang, Lei [1 ]
机构：
[1] Northeast Forestry Univ, Coll Chem Chem Engn & Resource Utilizat, Key Lab Forest Plant Ecol, Harbin 150040, Peoples R China
[2] Yunnan Acad Agr Sci, Agroprod Proc Res Inst, Kunming 650223, Peoples R China
[3] Northeast Forestry Univ, Sch Forestry, Harbin 150040, Peoples R China
来源：
SUSTAINABLE CHEMISTRY AND PHARMACY | 2025年 / 43卷
基金：
中国国家自然科学基金;
关键词：
Natural deep eutectic solvent; Liquidambar formosana; Essential oils; Microwave simultaneous hydrodistillation; Hydrolysis; And extraction; SIMULTANEOUS DISTILLATION; TANNINS; ANTIBACTERIAL; ELLAGITANNINS; METABOLISM; BARK;
D O I：
10.1016/j.scp.2024.101870
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this study, an improved method of naturally acidic deep eutectic solvent-mediated microwaveassisted simultaneous hydrodistillation, hydrolysis, and extraction (MSHDHE) was employed to obtain essential oils, gallic acid and ellagic acid from Liquidambar formosana leaves and fruits. The obtained target analytes were then analyzed via GC-MS and HPLC. The optimal extraction conditions were identified via a Box-Behnken design. Compared with fruits, L. formosana leaves contain more gallic acid and ellagic acid, which have more essential oils. GC-MS analysis revealed few variations in the composition and content of L. formosana leaves and fruit essential oils. A total of 36 components in the essential oil of L. formosana leaves and 55 components in the essential oil of the fruits were detected via GC-MS. Compared with classical hydrodistillation and microwave-assisted hydrodistillation, natural acidic deep eutectic solvents outperform conventional extraction solvents (pure water), providing a scientific foundation for the extraction of natural acid deep eutectic solvents consisting of choline chloride and natural organic acids.
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页数：18
相关论文
共 51 条
[1]   Deep eutectic solvents formed between choline chloride and carboxylic acids: Versatile alternatives to ionic liquids [J].
Abbott, AP ;
Boothby, D ;
Capper, G ;
Davies, DL ;
Rasheed, RK .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2004, 126 (29) :9142-9147
[2]   Novel solvent properties of choline chloride/urea mixtures [J].
Abbott, AP ;
Capper, G ;
Davies, DL ;
Rasheed, RK ;
Tambyrajah, V .
CHEMICAL COMMUNICATIONS, 2003, (01) :70-71
[3]   Optimization of ultrasonic-assisted extraction of antioxidant compounds from blackberry leaves using response surface methodology [J].
Aybastier, Onder ;
Isik, Esra ;
Sahin, Saliha ;
Demir, Cevdet .
INDUSTRIAL CROPS AND PRODUCTS, 2013, 44 :558-565
[4]   Isolation of essential oil from the leaves of Polygonum viscosum Such-ham. using microwave-assisted enzyme pretreatment followed by microwave hydrodistillation concatenated with liquid-liquid extraction [J].
Chen, Fengli ;
Jia, Jia ;
Zhang, Qiang ;
Yang, Lei ;
Gu, Huiyan .
INDUSTRIAL CROPS AND PRODUCTS, 2018, 112 :327-341
[5]   An improved approach for the isolation of essential oil from the leaves of Cinnamomum longepaniculatum using microwave-assisted hydrodistillation concatenated double-column liquid-liquid extraction [J].
Chen, Fengli ;
Xu, Ming ;
Yang, Xinyu ;
Liu, Junling ;
Xiao, Yao ;
Yang, Lei .
SEPARATION AND PURIFICATION TECHNOLOGY, 2018, 195 :110-120
[6]   A new approach for preparation of essential oil, followed by chlorogenic acid and hyperoside with microwave-assisted simultaneous distillation and dual extraction (MSDDE) from Vaccinium uliginosum leaves [J].
Chen, Fengli ;
Du, Xinqi ;
Zu, Yuangang ;
Yang, Lei .
INDUSTRIAL CROPS AND PRODUCTS, 2015, 77 :809-826
[7]   A novel approach for isolation of essential oil from fresh leaves of Magnolia sieboldii using microwave-assisted simultaneous distillation and extraction [J].
Chen, Fengli ;
Zu, Yuangang ;
Yang, Lei .
SEPARATION AND PURIFICATION TECHNOLOGY, 2015, 154 :271-280
[8]  
Chinese Pharmacopoeia Commission, 2020, Pharmacopoeia of the People's Republic of China, P264
[9]   Are Natural Deep Eutectic Solvents the Missing Link in Understanding Cellular Metabolism and Physiology? [J].
Choi, Young Hae ;
van Spronsen, Jaap ;
Dai, Yuntao ;
Verberne, Marianne ;
Hollmann, Frank ;
Arends, Isabel W. C. E. ;
Witkamp, Geert-Jan ;
Verpoorte, Robert .
PLANT PHYSIOLOGY, 2011, 156 (04) :1701-1705
[10]   CO2-supercritical extraction, hydrodistillation and steam distillation of essential oil of rosemary (Rosmarinus officinalis) [J].
Conde-Hernandez, Lilia A. ;
Espinosa-Victoria, Jose R. ;
Trejo, Arturo ;
Guerrero-Beltran, Jose A. .
JOURNAL OF FOOD ENGINEERING, 2017, 200 :81-86
123456